Reference Friedel-Crafts Acylation of m-Xylene with Phthalic Anhydride, Experimental Organic Chemistry, Gilbert and Martin, 5th Edition, 2011, p. 505-506. Health & Safety Evaluation Chemical Name Amount per 100 Aldrich Catalog # students (g or mL) EH&S Phthalic anhydride 50 g 320064 Aluminum chloride, anhydrous 100 g 237051 m-xylene 300 mL 185566 Hydrochloric acid, conc. 100 mL 320331 * Water 500 mL n/a * Diethyl ether 1400 mL 346136 Hydrochloric acid, 6M 250 mL 320331 Sodium sulfate 500 g 239313
Reference Friedel-Crafts Acylation of m-Xylene with Phthalic Anhydride, Experimental Organic Chemistry, Gilbert and Martin, 5th Edition, 2011, p. 505-506. Health & Safety Evaluation Chemical Name Aldrich Catalog # Amount per 100 students (g or mL) EH&S Phthalic anhydride 320064 50 g Aluminum chloride, anhydrous 237051 100 g m-xylene 185566 300 mL Hydrochloric acid, conc. 320331 100 mL * Water n/a 500 mL Diethyl ether 346136 1400 mL * Hydrochloric acid, 6M 320331 250 mL Sodium sulfate 239313 500 g
a_guide_to_green_chemistry_experiments_for_undergraduate_organic_chemistry_labs_march_2018_v2p.docx