2-(5-Chloro-2-thienyl)- 4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1i) S30 2-(2-Biphenyl-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1j) S33 2-(4-Methoxy-2-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1k) S36 2-Isopropyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1l) S39 2-(Tert-butyl)-4,4,5,5-tetramthyl-1,3,2-dioxaborolane (1m S42 1H and 13C spectrum of Isolated MgBr2/THF Solid (Scheme 2) 1H NMR of Isolated Solid S45 13C NMR of Isolated Solid S46
2-(5-Chloro-2-thienyl)- 4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1i) 2-(2-Biphenyl-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1j) 2-(4-Methoxy-2-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1k) 2-Isopropyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1l) 2-(Tert-butyl)-4,4,5,5-tetramthyl-1,3,2-dioxaborolane (1m 1H and 13C spectrum of Isolated MgBr2/THF Solid (Scheme 2) 1H NMR of Isolated Solid 13C NMR of Isolated Solid S30 S33 S36 S39 S42 S45 S46
1-s2.0-S0040403914020875-mmc1.docx