xxx→yyy yy m/z (quantitation) zz Analyte 1 Matrix 1 xx xxx→yyy m/z yy (confirmation) zz Analyte 1 Matrix 2 xx xxx→yyy m/z yy (confirmation) zz Analyte 1 Matrix 3 xx xxx→yyy m/z yy (confirmation) zz Analyte 2 Matrix 1 xx xxx→yyy m/z yy (confirmation) zz Analyte 2 Matrix 2 xx xxx→yyy m/z yy (confirmation) zz Analyte 2 Matrix 3 xx xxx→yyy m/z yy (confirmation) zz Analytical Method [Method ID] was [successfully/not successfully] validated by an independent a laboratory and/or personnel unfamiliar with the method. Samples of [matrices] were spiked with [analytes] at levels ranging from [xx] to [yy] ppm. Recovery of analytes from spiked samples ranged from [xx] to [yy]% with a maximum relative standard deviation of [xx]% (Table B.5.2.2.1-4). Contact with the sponsor [was/was not] required and acceptable recoveries were obtained after [x] trials. The validating laboratory recommends the following revisions to the method: Revision 1 Revision 2 Etc. B.5.2.2.1-4. Accuracy and Precision Data for the Independent Laboratory Validation of [Method ID] for Livestock Matrices. Fortification Independent Laboratory Validation Recovery (%) RSD Analyte Matrix (ppm) (%) Individual Mean Analyte 1 Matrix 1 xx xxx→yyy m/z yy (quantitation) zz Analyte 1 Matrix 2 xx xxx→yyy m/z yy (quantitation) zz Analyte 1 Matrix 3 xx xxx→yyy m/z yy (quantitation) zz Analyte 2 Matrix 1 xx xxx→yyy m/z yy (quantitation) zz Analyte 2 Matrix 2 xx xxx→yyy m/z yy (quantitation) zz Analyte 2 Matrix xx 3
m/z xxx→yyy (quantitation) yy zz Analyte 1 m/z xxx→yyy (confirmation) Matrix 1 xx yy zz Analyte 1 m/z xxx→yyy (confirmation) Matrix 2 xx yy zz Analyte 1 m/z xxx→yyy (confirmation) Matrix 3 xx yy zz Analyte 2 m/z xxx→yyy (confirmation) Matrix 1 xx yy zz Analyte 2 m/z xxx→yyy (confirmation) Matrix 2 xx yy zz Analyte 2 m/z xxx→yyy (confirmation) Matrix 3 xx yy zz Analytical Method [Method ID] was [successfully/not successfully] validated by an independent a laboratory and/or personnel unfamiliar with the method. Samples of [matrices] were spiked with [analytes] at levels ranging from [xx] to [yy] ppm. Recovery of analytes from spiked samples ranged from [xx] to [yy]% with a maximum relative standard deviation of [xx]% (Table B.5.2.2.1-4). Contact with the sponsor [was/was not] required and acceptable recoveries were obtained after [x] trials. The validating laboratory recommends the following revisions to the method: Revision 1 Revision 2 Etc. B.5.2.2.1-4. Accuracy and Precision Data for the Independent Laboratory Validation of [Method ID] for Livestock Matrices. Analyte Matrix Fortification (ppm) Independent Laboratory Validation Recovery (%) RSD (%) Individual Mean Analyte 1 m/z xxx→yyy (quantitation) Matrix 1 xx yy zz Analyte 1 m/z xxx→yyy (quantitation) Matrix 2 xx yy zz Analyte 1 m/z xxx→yyy (quantitation) Matrix 3 xx yy zz Analyte 2 m/z xxx→yyy (quantitation) Matrix 1 xx yy zz Analyte 2 m/z xxx→yyy (quantitation) Matrix 2 xx yy zz Analyte 2 Matrix 3 xx
b.5.2_residue_analytical_methods.docx