Reference The Oxidation of a Ketone to a Carboxylic Acid: Cyclohexanone from Cyclohexanol, Macroscale and Microscale Organic Experiments, Williamson, K.L., Masters, K.M., 6th Edition, Brooks/Cole Cengage Learning, 2011, pp. 358-359. Health & Safety Evaluation Amount per Chemical Name 100 students Aldrich Catalog # (g or mL) EH&S Sodium dichromate dihydrate 375 g 398063 * Acetic acid, 1M 1000 mL 965092 Cyclohexanol 375 g 105899 Water 2500 mL n/a Sodium chloride 400 g 746398 * Anhydrous diethyl ether 750 mL 346136 Sodium hydroxide, 3M 500 mL 221465 Sodium chloride, sat. solution 750 mL
Reference The Oxidation of a Ketone to a Carboxylic Acid: Cyclohexanone from Cyclohexanol, Macroscale and Microscale Organic Experiments, Williamson, K.L., Masters, K.M., 6th Edition, Brooks/Cole Cengage Learning, 2011, pp. 358-359. Health & Safety Evaluation Chemical Name Aldrich Catalog # Amount per 100 students (g or mL) EH&S Sodium dichromate dihydrate 398063 375 g * Acetic acid, 1M 965092 1000 mL Cyclohexanol 105899 375 g Water n/a 2500 mL Sodium chloride 746398 400 g Anhydrous diethyl ether 346136 750 mL * Sodium hydroxide, 3M 221465 500 mL Sodium chloride, sat. solution 750 mL
a_guide_to_green_chemistry_experiments_for_undergraduate_organic_chemistry_labs_march_2018_v2p.docx