mT). Spectrum on right shows reaction between acetone oxime and PTAD with two new signals. ESI of PTAD + acetone reaction (removed from NMR tube and quickly diluted to 1 ng/uL in 50:50 water:acetonitrile 0.1% formic acid and injected into ESI-MS). Other products have begun to form as the nitroso decomposes. References to Supporting Information Ghorbani-Choghamarani, A.; Chenani, Z.; Mallakpour, S. Syn. Comm. 2009, 39, 4264-4270. Hall, J. H.; Bigard, W. E.; Fargher, J. M.; Jones, M. L. J. Org. Chem. 1982, 47, 1459-1462. Zolfigol, M. A.; Ghorbani-Vaghei, R.; Mallakpour, S.; Chehardoli, G.; A.; Yazdi, A. H. Synthesis 2006, 1631-1634.
mT). Spectrum on right shows reaction between acetone oxime and PTAD with two new signals. ESI of PTAD + acetone reaction (removed from NMR tube and quickly diluted to 1 ng/uL in 50:50 water:acetonitrile 0.1% formic acid and injected into ESI-MS). Other products have begun to form as the nitroso decomposes. References to Supporting Information Ghorbani-Choghamarani, A.; Chenani, Z.; Mallakpour, S. Syn. Comm. 2009, 39, 4264-4270. Hall, J. H.; Bigard, W. E.; Fargher, J. M.; Jones, M. L. J. Org. Chem. 1982, 47, 1459-1462. Zolfigol, M. A.; Ghorbani-Vaghei, R.; Mallakpour, S.; Chehardoli, G.; A.; Yazdi, A. H. Synthesis 2006, 1631-1634.
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