This section be taught before the A-level organic chemistry topics allowing the technique to be re-visited and to be part of practice questions throughout the teaching of the A-level organic topics. Time Learning activity with opportunity to Assessment Learning outcome Resources Learning objective taken develop skills opportunities Using 1H and 13C NMR to 2.0 RSC Spectral School: Predict the number, position, relative June 2013 Unit 4 Students should be able to: deduce information about intensity and splitting of signals in Question 7 understand the use of TMS the 1H NMR spectrum of compounds (QS13.4.07) the structure of organic RSC Spectroscopy and the δ scale for (AO2 - Apply knowledge and molecules. January 2013 Unit 4 resource: chemical shift understanding). Question 5 understand the use of Predict the number and position of (QS13.4.05) Understand similarities and Database of spectra for deuterated solvents or signals in the 13C NMR spectrum of June 2012 Unit 4 differences between 1H organic compounds CCl4 compounds (AO2 - Apply knowledge Question 8 and 13C NMR. use the n+1 rule to deduce and understanding). (QS12.4.08) CLEAPSS Spectra spin-spin splitting patterns Use data from NMR, and other January 2011 Unit 4 Understand the use of TMS (Secondary Science of adjacent, non-equivalent analytical methods on the Question 5 protons in aliphatic and suitable solvents. Guide L202) specification, to deduce the structure (QW11.4.05) compounds of compounds (AO2 - Apply January 2003 Unit 4 deduce the structure of (Subscription required) knowledge and understanding; Question 5 compounds using 1H NMR MS3.1 Translate information (QW03.4.05) to deduce structures between graphical, numerical and January 2002 Unit 4 including the number, algebraic forms). Question 4 position, relative intensity (QW02.4.04) and splitting of signals deduce the structure of compounds using 13C NMR to deduce structures including the number and position of signals.
This section be taught before the A-level organic chemistry topics allowing the technique to be re-visited and to be part of practice questions throughout the teaching of the A-level organic topics. Learning objective Time taken Learning outcome Learning activity with opportunity to develop skills Assessment opportunities Resources Using 1H and 13C NMR to deduce information about the structure of organic molecules. Understand similarities and differences between 1H and 13C NMR. Understand the use of TMS and suitable solvents. 2.0 Students should be able to: understand the use of TMS and the δ scale for chemical shift understand the use of deuterated solvents or CCl4 use the n+1 rule to deduce spin-spin splitting patterns of adjacent, non-equivalent protons in aliphatic compounds deduce the structure of compounds using 1H NMR to deduce structures including the number, position, relative intensity and splitting of signals deduce the structure of compounds using 13C NMR to deduce structures including the number and position of signals. Predict the number, position, relative intensity and splitting of signals in the 1H NMR spectrum of compounds (AO2 - Apply knowledge and understanding). Predict the number and position of signals in the 13C NMR spectrum of compounds (AO2 - Apply knowledge and understanding). Use data from NMR, and other analytical methods on the specification, to deduce the structure of compounds (AO2 - Apply knowledge and understanding; MS3.1 Translate information between graphical, numerical and algebraic forms). June 2013 Unit 4 Question 7 (QS13.4.07) January 2013 Unit 4 Question 5 (QS13.4.05) June 2012 Unit 4 Question 8 (QS12.4.08) January 2011 Unit 4 Question 5 (QW11.4.05) January 2003 Unit 4 Question 5 (QW03.4.05) January 2002 Unit 4 Question 4 (QW02.4.04) RSC Spectral School: RSC Spectroscopy resource: Database of spectra for organic compounds CLEAPSS Spectra (Secondary Science Guide L202) (Subscription required)
AQA-7405-SOW.DOCX