Introduction: Procedure: (Reference: use proper format. Any Changes/Modifications?) Procedure for the Fisher esterification of acetic acid with isoamyl alcohol. Procedural Step Observations/Comments/Inferences Record amounts of reagents used. Table 10.1 Table of Reagents for Experiment 10 Fisher Esterification. Reagent Formula Mwt. d Mp* Bp* Haz. Properties (g/mol) (g/ml) (C) (C) Acetic acid, glacial (conc.) 17.4 M Isoamyl alcohol 88.15 130 Irritant H (3-methyl -1-butanol) Sulfuric acid, conc. H2SO4 1.840 18 M Distilled water H2O 18.02 1.000 0 100 none Diethyl ether 5% sodium carbonate (aq) Na2CO3 (aq) Sat. sodium chloride (aq) NaCl (aq) (brine) Calcium chloride (anhydr) CaCl2 acetone, wash
Introduction: Procedure: (Reference: use proper format. Any Changes/Modifications?) Procedure for the Fisher esterification of acetic acid with isoamyl alcohol. Procedural Step Observations/Comments/Inferences Record amounts of reagents used. Table 10.1 Table of Reagents for Experiment 10 Fisher Esterification. Reagent Formula Mwt. (g/mol) d (g/ml) Mp* (C) Bp* (C) Haz. Properties Acetic acid, glacial (conc.) 17.4 M Isoamyl alcohol (3-methyl -1-butanol) 88.15 130 Irritant Sulfuric acid, conc. 18 M H2SO4 1.840 Distilled water H2O 18.02 1.000 0 100 none Diethyl ether 5% sodium carbonate (aq) Na2CO3 (aq) Sat. sodium chloride (aq) (brine) NaCl (aq) Calcium chloride (anhydr) CaCl2 acetone, wash H
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