4 2H pattern 7.5  &8.1 5 1H xchanges 10.6  with D2O Unknown # 360-14-19 Mol. Wt. = 59.11 g/mol Chemical Formula = C3H9N Degrees of Unsaturation = ___________________________________ b.p. = 47.8C IR Spectra (liquid film on KBr Disc) 1H-NMR Spectra (at 90 MHz in CDCl3) Infrared Spectra (liquid film on KBr disc): 1H-NMR Integration Data: (at 90 MHz in CDCl3) Spectrum Absorp'n Frequency Peak Shape Peak Intensity Functional Group Signal Shift Integrat'n Splitting Comment Signal Band # (cm-1) (sharp, broad) (strong, med. Indicated # H Assignment Region or weak) 1 3H 0.92  2 2H xchanges  1.24 with D2O 3 2H  4 2H 2.65  Unknown # 360-14-20 Mol. Wt. = 107.16 g/mol Chemical Formula = C7H9N Degrees of Unsaturation = ___________________________________ b.p. = 200.5C IR Spectra (on KBr Disc) 1H-NMR Spectra (at 400 MHz in CDCl3) Infrared Spectra (on KBr disc): 1H-NMR Integration Data: (at 400 MHz in CDCl3) Spectrum Absorp'n Frequency Peak Shape Peak Intensity Functional Group Signal Shift Integrat'n Splitting Comment Signal Band # (cm-1) (sharp, broad) (strong, med. Indicated # H Assignment Region or weak) 1 3H 2.2  2 2H xchanges  3.5 with D2O 3 2H  4 2H 6.95 
pattern 4  7.5 &8.1 2H 5  10.6 1H xchanges with D2O Unknown # 360-14-19 Mol. Wt. = 59.11 g/mol Chemical Formula = C3H9N Degrees of Unsaturation = ___________________________________ b.p. = 47.8C IR Spectra (liquid film on KBr Disc) 1H-NMR Spectra (at 90 MHz in CDCl3) Infrared Spectra (liquid film on KBr disc): 1H-NMR Integration Data: (at 90 MHz in CDCl3) Spectrum Region Absorp'n Band # Frequency (cm-1) Peak Shape (sharp, broad) Peak Intensity (strong, med. or weak) Functional Group Indicated Signal # Shift Integrat'n Splitting Comment H Signal Assignment 1  0.92 3H 2  1.24 2H xchanges with D2O 3  2H 4  2.65 2H Unknown # 360-14-20 Mol. Wt. = 107.16 g/mol Chemical Formula = C7H9N Degrees of Unsaturation = ___________________________________ b.p. = 200.5C IR Spectra (on KBr Disc) 1H-NMR Spectra (at 400 MHz in CDCl3) Infrared Spectra (on KBr disc): 1H-NMR Integration Data: (at 400 MHz in CDCl3) Spectrum Region Absorp'n Band # Frequency (cm-1) Peak Shape (sharp, broad) Peak Intensity (strong, med. or weak) Functional Group Indicated Signal # Shift Integrat'n Splitting Comment H Signal Assignment 1  2.2 3H 2  3.5 2H xchanges with D2O 3  2H 4  6.95 2H
360RptBk_12.docx