Region Band # (cm-1) (sharp, broad) (strong, med. Indicated # H Assignment or weak) 1 6H 1.4  2 3H  2.2 3 1H xchanges  with D2O Unknown # 360-14-6 Mol. Wt. = 104.15 g/mol Chemical Formula = C8H8 Degrees of Unsaturation = ___________________________________ b.p. = 146C IR Spectra (liquid film (neat) on KBr Disc) 1H-NMR Spectra (at 90 MHz in CDCl3) Infrared Spectra (liquid film (neat) on KBr disc): 1H-NMR Integration Data: (at 90 MHz in CDCl3) Spectrum Absorp'n Frequency Peak Shape Peak Intensity Functional Group Signal Shift Integrat'n Splitting Comment Signal Band # (cm-1) (sharp, broad) (strong, med. Indicated # H Assignment Region or weak) 1 1H 5.2  2 1H 5.7  3 1H  4 5H  7.3 Unknown # 360-14-7 Mol. Wt. = 121.18 g/mol Chemical Formula = C8H11N Degrees of Unsaturation = ___________________________________ b.p. = 210C IR Spectra (liquid film (neat) on KBr Disc) 1H-NMR Spectra (at 90 MHz 10.5 mol% in CDCl3) Infrared Spectra (liquid film (neat) on KBr disc): 1H-NMR Integration Data: (at 90 MHz 10.5 mol% in CDCl3) Spectrum Absorp'n Frequency Peak Shape Peak Intensity Functional Group Signal Shift Integrat'n Splitting Comment Signal Band # (cm-1) (sharp, broad) (strong, med. Indicated # H Assignment Region or weak) 1 3H  1.2 2 2H 2.46 
Region Band # (cm-1) (sharp, broad) (strong, med. or weak) Indicated # H Assignment 1  1.4 6H 2  2.2 3H 3  1H xchanges with D2O Unknown # 360-14-6 Mol. Wt. = 104.15 g/mol Chemical Formula = C8H8 Degrees of Unsaturation = ___________________________________ b.p. = 146C IR Spectra (liquid film (neat) on KBr Disc) 1H-NMR Spectra (at 90 MHz in CDCl3) Infrared Spectra (liquid film (neat) on KBr disc): 1H-NMR Integration Data: (at 90 MHz in CDCl3) Spectrum Region Absorp'n Band # Frequency (cm-1) Peak Shape (sharp, broad) Peak Intensity (strong, med. or weak) Functional Group Indicated Signal # Shift Integrat'n Splitting Comment H Signal Assignment 1  5.2 1H 2  5.7 1H 3  1H 4  7.3 5H Unknown # 360-14-7 Mol. Wt. = 121.18 g/mol Chemical Formula = C8H11N Degrees of Unsaturation = ___________________________________ b.p. = 210C IR Spectra (liquid film (neat) on KBr Disc) 1H-NMR Spectra (at 90 MHz 10.5 mol% in CDCl3) Infrared Spectra (liquid film (neat) on KBr disc): 1H-NMR Integration Data: (at 90 MHz 10.5 mol% in CDCl3) Spectrum Region Absorp'n Band # Frequency (cm-1) Peak Shape (sharp, broad) Peak Intensity (strong, med. or weak) Functional Group Indicated Signal # Shift Integrat'n Splitting Comment H Signal Assignment 1  1.2 3H 2  2.46 2H
360RptBk_12.docx