26600 SCHEDULE OF EXPERIMENTS, Spring 2014 Week(s) WEEK of: EXPERIMENT REFERENCE # Check In Handout #1, 1 Synthesis of Fruit Fragrances 1/13 Experiment #1 (Fischer Esterification) Experiment 22B, Williamson Ether Synthesis: 2 1/20 pages 321-311 (Preparation of Methyl p-ethylphenyl Ether) Diels Alder Reaction Experiment 14, 3 1/27 (4-Cyclohexene-cis-1,2-dicarboxylic Acid Anhydride) pages 257-2691 Handout #4, Electrophilic Aromatic Substitution 4 Experiment #4 2/3 (Friedel-Crafts Acylation of 2-Chlorotoluene) Handout #5, Green Cross-coupling Reaction 5 2/10 Experiment #5 (Suzuki Coupling in Aqueous Media) 2/17 Qualitative Analysis Handout #6, 6 - 9 through (Separation, Purification, Experiment #6 3/10 and Characterization, of Unknowns) 10 Spring Break 3/17 Handout #7, Stereochemistry of the Wittig Reaction 11 3/24 Experiment #7 (Influence of a Spectator Ion) Chemoselective Reduction of 3-Nitroacetophenone Handout #8, 12 3/31 (A Compound with two Reducible Groups) Experiment #8 4/7 Handout #9, Synthesis Project 13 and 14 and Experiment #9 (Chalcone Synthesis Michael addition/Aldol Condensation) – 4/14 Evaluation of L-Proline as a Catalyst for an 15 4/21 Handout #10, Asymmetric Aldol Reaction
26600 SCHEDULE OF EXPERIMENTS, Spring 2014 WEEK # Week(s) of: EXPERIMENT REFERENCE 1 1/13 Check In Synthesis of Fruit Fragrances (Fischer Esterification) Handout #1, Experiment #1 2 1/20 Williamson Ether Synthesis: (Preparation of Methyl p-ethylphenyl Ether) Experiment 22B, pages 321-311 3 1/27 Diels Alder Reaction (4-Cyclohexene-cis-1,2-dicarboxylic Acid Anhydride) Experiment 14, pages 257-2691 4 2/3 Electrophilic Aromatic Substitution (Friedel-Crafts Acylation of 2-Chlorotoluene) Handout #4, Experiment #4 5 2/10 Green Cross-coupling Reaction (Suzuki Coupling in Aqueous Media) Handout #5, Experiment #5 6 - 9 2/17 through 3/10 Qualitative Analysis (Separation, Purification, and Characterization, of Unknowns) Handout #6, Experiment #6 10 3/17 Spring Break 11 3/24 Stereochemistry of the Wittig Reaction (Influence of a Spectator Ion) Handout #7, Experiment #7 12 3/31 Chemoselective Reduction of 3-Nitroacetophenone (A Compound with two Reducible Groups) Handout #8, Experiment #8 13 and 14 4/7 and 4/14 Synthesis Project (Chalcone Synthesis – Michael addition/Aldol Condensation) Handout #9, Experiment #9 15 4/21 Evaluation of L-Proline as a Catalyst for an Asymmetric Aldol Reaction Handout #10,
26600%20SCHEDULE%20Spring%202014.docx