90 α/° 92.466(7) β/° 90 γ/° Volume/Å3 1816.7(7) Z 2 2.688 ρcalcg/cm3 11.549 μ/mm1 F(000) 1352.0 Crystal size/mm3 0.425 × 0.258 × 0.158 Radiation MoKα (λ = 0.71073) 2Θ range for data collection/° 5.944 to 82.904 -17 h 17, -17 k 17, -36 l ≤ ≤ ≤ ≤ ≤ ≤ Index ranges 37 Reflections collected 111312 11803 [Rint = 0.0590, Rsigma = Independent reflections 0.0374] Data/restraints/parameters 11803/0/165 Goodness-of-fit on F2 1.255 Final R indexes [I>=2σ (I)] R1 = 0.0664, wR2 = 0.1040 Final R indexes [all data] R1 = 0.0829, wR2 = 0.1093 Largest diff. peak/hole / e Å-3 1.67/-2.17 Figure 10 Thermal ellipsoid plot (50% probability surface) of the asymmetric unit of 10[SnBr3]. Hydrogen atoms are omitted for clarity. Table 10 Summary of crystallographic data and refinement details for 10[SnBr3] Identification code AMS50 Empirical formula C10H22Br4O5Sn2 Formula weight 779.29 Temperature/K 143.21 Crystal system monoclinic Space group P21/c a/Å 13.9519(11) b/Å 11.5896(9) c/Å 13.0100(11) 90 α/° 94.593(3) β/° 90 γ/° Volume/Å3 2096.9(3) Z 4 2.468 ρcalcg/cm3 10.017 μ/mm1 F(000) 1448.0 Crystal size/mm3 0.388 × 0.306 × 0.055 Radiation MoKα (λ = 0.71073) 2Θ range for data collection/° 5.858 to 72.856 -22 h 23, -19 k 19, -21 l ≤ ≤ ≤ ≤ ≤ ≤ Index ranges 21
α/° 90 β/° 92.466(7) γ/° 90 Volume/Å3 1816.7(7) Z 2 ρcalcg/cm3 2.688 μ/mm1 11.549 F(000) 1352.0 Crystal size/mm3 0.425 × 0.258 × 0.158 Radiation MoKα (λ = 0.71073) 2Θ range for data collection/° 5.944 to 82.904 Index ranges -17 ≤ h ≤ 17, -17 ≤ k ≤ 17, -36 ≤ l ≤ 37 Reflections collected 111312 Independent reflections 11803 [Rint = 0.0590, Rsigma = 0.0374] Data/restraints/parameters 11803/0/165 Goodness-of-fit on F2 1.255 Final R indexes [I>=2σ (I)] R1 = 0.0664, wR2 = 0.1040 Final R indexes [all data] R1 = 0.0829, wR2 = 0.1093 Largest diff. peak/hole / e Å-3 1.67/-2.17 Figure 10 Thermal ellipsoid plot (50% probability surface) of the asymmetric unit of 10[SnBr3]. Hydrogen atoms are omitted for clarity. Table 10 Summary of crystallographic data and refinement details for 10[SnBr3] Identification code AMS50 Empirical formula C10H22Br4O5Sn2 Formula weight 779.29 Temperature/K 143.21 Crystal system monoclinic Space group P21/c a/Å 13.9519(11) b/Å 11.5896(9) c/Å 13.0100(11) α/° 90 β/° 94.593(3) γ/° 90 Volume/Å3 2096.9(3) Z 4 ρcalcg/cm3 2.468 μ/mm1 10.017 F(000) 1448.0 Crystal size/mm3 0.388 × 0.306 × 0.055 Radiation MoKα (λ = 0.71073) 2Θ range for data collection/° 5.858 to 72.856 Index ranges -22 ≤ h ≤ 23, -19 ≤ k ≤ 19, -21 ≤ l ≤ 21
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