7 hours Solving spectroscopic Main chemical ideas: structural analysis problems using a range of Finally, aspirin discussed Carbon-13 NMR is new content. Introductory – data (HSW 2). in WM is revisited as the notes can be found on websites such as , , – context for a more detailed Solving advanced and . discussion of mass spectroscopic problems All carbon-13 NMR spectra that are assessed spectrometry, as well as using a range of data (HSW will be proton decoupled (i.e. unsplit introduction of proton and 5). For proton NMR, explanation of splitting carbon-13 NMR and the There are many examples patterns up to quartets using the + 1’ rule is ‘n use of combined of spectra available at . required; further explanation of splitting is not techniques in structural required. analysis. Spectroscopic analysis offers opportunities for many different types of teaching, including individual and group-work, and The Oceans (O) – Specification reference & Suggested Delivery Guides Suggested practicals, PAGs. Notes statements teaching time HSW and maths skills ideas.
Finally, aspirin – discussed in WM – is revisited as the context for a more detailed discussion of mass spectrometry, as well as introduction of proton and carbon-13 NMR and the use of combined techniques in structural analysis. 7 hours Solving spectroscopic problems using a range of data (HSW 2). Solving advanced spectroscopic problems using a range of data (HSW 5). There are many examples of spectra available at . Main chemical ideas: structural analysis Carbon-13 NMR is new content. Introductory notes can be found on websites such as , , and . All carbon-13 NMR spectra that are assessed will be proton decoupled (i.e. unsplit For proton NMR, explanation of splitting patterns up to quartets using the ‘n + 1’ rule is required; further explanation of splitting is not required. Spectroscopic analysis offers opportunities for many different types of teaching, including individual and group-work, and The Oceans (O) – Specification reference & statements Suggested teaching time Delivery Guides Suggested practicals, PAGs. HSW and maths skills ideas. Notes
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