N-((5-bromo-2-hydroxyphenyl)(2,5-dimethoxyphenyl)methyl)acetamide (9) IR (KBr, cm-1): 3372, 3267, 2854, 1652; 1H NMR (400 MHz, DMSO-d6): (ppm) 1.82 (s, 3H), δ 3.31 (s, 3H), 3.76 (s, 3H), 6.30 (d, = 6 Hz, 1H), 6.69 (d, = 8.4 Hz, 1H), J J 6.87 (d, = 6.4 Hz, 1H), 7.09-7.28 (m, 4H), 8.50 (d, = 9.2 Hz, 1H), 9.35 (s, 1H) ppm; J J 13CNMR (100 MHz; DMSO-d6) (ppm) 23.12, 41.05, 50.46, 115.68, 126.26, 127.32, 128.33, δ 128.48, 128.79, 128.96, 129.05, 131.78, 141.55, 142.32, 152.94, 168.75; MS: = 380 (M+). m/z
N-((5-bromo-2-hydroxyphenyl)(2,5-dimethoxyphenyl)methyl)acetamide (9) IR (KBr, cm-1): 3372, 3267, 2854, 1652; 1H NMR (400 MHz, DMSO-d6): δ (ppm) 1.82 (s, 3H), 3.31 (s, 3H), 3.76 (s, 3H), 6.30 (d, J = 6 Hz, 1H), 6.69 (d, J = 8.4 Hz, 1H), 6.87 (d, J = 6.4 Hz, 1H), 7.09-7.28 (m, 4H), 8.50 (d, J = 9.2 Hz, 1H), 9.35 (s, 1H) ppm; 13CNMR (100 MHz; DMSO-d6) δ (ppm) 23.12, 41.05, 50.46, 115.68, 126.26, 127.32, 128.33, 128.48, 128.79, 128.96, 129.05, 131.78, 141.55, 142.32, 152.94, 168.75; MS: m/z = 380 (M+).
cjc-2015-0230-supplement-1.docx