Chemdraw and Table templates Scheme 1.1 Synthesis of catalyst 4 O N O 2. NEt3 (2.5 eq.) CO2H H 0 °C to rt, 12 h N Bn 3 (56%) N O Cl PhMe, 80 °C 1. SOCl2, 80 °C, O 16 h N Bn 2 h H 2 (1.0 eq.) 1 O 4 (80%) N Bn Scheme 1.2 Methylation of catalyst 4 O MeI (4.0 eq.) N O 4 THF, 30 °C, 16 h N Bn 5 (99%)
Chemdraw and Table templates Scheme 1.1 Synthesis of catalyst 4 CO2H Cl 1. SOCl2, 80 °C, 2 h 2. NEt3 (2.5 eq.) 0 °C to rt, 12 h N O N O Bn 3 (56%) H PhMe, 80 °C 16 h O N O N Bn 1 O N Bn H 2 (1.0 eq.) 4 (80%) Scheme 1.2 Methylation of catalyst 4 MeI (4.0 eq.) 4 THF, 30 °C, 16 h O N O N Bn 5 (99%)
Confirmation_Report_Template.docx