~1 minute and then click start measurement scan will take some time depending on the angles scanned and scan speed data is automatically saved into a .raw file This needs to be opened in the Jade software, and can then be saved as a normal .txt file Do not anything in the Jade software as it actually “delete” deletes the original file!!! It does not simply remove it from the program. the X-ray off (button on front) the power switch in the back from the computer the cooling system run for a couple minutes after turning the X-ray off off the cooling system the power strip and wheel the system back to its normal location down the computer spectrum acquired from the silicon on tape with a disk sample holder:The circled peaks are extra and not from Si. They are most likely from the sample holder. There is also a missing peak around 68 degrees which could be due to the thin layer of powder and possibly some preferred orientation of the powder.
~1 minute and then click start measurement scan will take some time depending on the angles scanned and scan speed data is automatically saved into a .raw file This needs to be opened in the Jade software, and can then be saved as a normal .txt file Do not “delete” anything in the Jade software as it actually deletes the original file!!! It does not simply remove it from the program. the X-ray off (button on front) the power switch in the back from the computer the cooling system run for a couple minutes after turning the X-ray off off the cooling system the power strip and wheel the system back to its normal location down the computer spectrum acquired from the silicon on tape with a disk sample holder:The circled peaks are extra and not from Si. They are most likely from the sample holder. There is also a missing peak around 68 degrees which could be due to the thin layer of powder and possibly some preferred orientation of the powder.
Rigaku-SOP-1.docx