Gas Analysis: a) Thermal conductivity method. b) Heat of Reaction method. Oxygen Analysis: a) Magneto Dynamic instrument(Pauling cell) b) Thermomagnetic type or Hot wire type instrument. c) Zirconia oxygen analyzer. d) Mackerth type galvanic analyzer for dissolved oxygen analysis. Liquid analysis: a) Electrodes-Ion selective, Molecular selective types- their variations. b) pH analysis: pH electrodes, circuit for pH measurement and applications. c) Conductivity cells standards, circuits. – d) Polarography- apparatus, circuits and techniques-pulse polarography, applications e) Colorimetry. Spectroscopic Methods : Introduction, Laws relating to absorption of radiation,Molecular Absorption Spectroscopy in UV & VIS ranges: sources, wavelength selectors, sample container, detectors, Spectrophotometers (Single beam & Dual beam arrangement). Atomic Absorption & Emission spectroscopy : Atomizers, sources, single & dual beam arrangement Plasma Spectroscopy : Sequential & Simultaneous multichannel Instruments. Atomic X Ray spectrometry: Absorption & diffraction phenomena, sources, detectors, techniques. IR Spectroscopy: sources, monochromators, detectors. IR Spectrometer, FT-IR spectrometers. Chromatography: Introduction, basic definitions, some relationships. Gas chromatography: basic parts, columns, detectors, techniques. LC: types, HPLC : basic parts, sample injection system, column, detectors, Applications. BEYOND SYLLABI COVERAGE LECTURE PLAN Sl. Modules/Sub Topics Required Books/Study Materials Proposed No. Lectures Introduction to Analytical Khandpur / 01 1 Patranabis/ Instrumentation Difference between Note . analytical and other instruments. Classification, types of Instrumental methods. Measurement of Humidity: Dry & wet 02 1 Patranabis/Note. psychrometer, Hair hygrometer, Measurement of Humidity: electrical 04 1 Patranabis/Note type, Electrolysis type hygrometer, Dew point meter. Moisture: Electrical conductivity type, 05 1 Patranabis/Note Capacitive method type, IR method, Microwave method, Crystal oscillator method. Viscosity: Poiseuilles formula, 06 1 Patranabis/Note
Gas Analysis: a) Thermal conductivity method. b) Heat of Reaction method. Oxygen Analysis: a) Magneto Dynamic instrument(Pauling cell) b) Thermomagnetic type or Hot wire type instrument. c) Zirconia oxygen analyzer. d) Mackerth type galvanic analyzer for dissolved oxygen analysis. Liquid analysis: a) Electrodes-Ion selective, Molecular selective types- their variations. b) pH analysis: pH electrodes, circuit for pH measurement and applications. c) Conductivity cells – standards, circuits. d) Polarography- apparatus, circuits and techniques-pulse polarography, applications e) Colorimetry. Spectroscopic Methods : Introduction, Laws relating to absorption of radiation,Molecular Absorption Spectroscopy in UV & VIS ranges: sources, wavelength selectors, sample container, detectors, Spectrophotometers (Single beam & Dual beam arrangement). Atomic Absorption & Emission spectroscopy : Atomizers, sources, single & dual beam arrangement Plasma Spectroscopy : Sequential & Simultaneous multichannel Instruments. Atomic X Ray spectrometry: Absorption & diffraction phenomena, sources, detectors, techniques. IR Spectroscopy: sources, monochromators, detectors. IR Spectrometer, FT-IR spectrometers. Chromatography: Introduction, basic definitions, some relationships. Gas chromatography: basic parts, columns, detectors, techniques. LC: types, HPLC : basic parts, sample injection system, column, detectors, Applications. BEYOND SYLLABI COVERAGE LECTURE PLAN Sl. No. Modules/Sub Topics Required Lectures Books/Study Materials Proposed 01 Introduction to Analytical Instrumentation Difference between analytical and other instruments. Classification, types of Instrumental methods. 1 Patranabis/ Khandpur / Note . 02 Measurement of Humidity: Dry & wet psychrometer, Hair hygrometer, 1 Patranabis/Note. 04 Measurement of Humidity: electrical type, Electrolysis type hygrometer, Dew point meter. 1 Patranabis/Note 05 Moisture: Electrical conductivity type, Capacitive method type, IR method, Microwave method, Crystal oscillator method. 1 Patranabis/Note 06 Viscosity: Poiseuilles formula, 1 Patranabis/Note
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