Annex-IX FORMAT FOR PERFORMACE SHEET LINEARITY, REPEATABILITY & REPRODUCIBILITY TEST A) Linearity details: Name of analyte: Chloramphenicol Date:.................. Start Time:...................End Time:.................. Obtained Area Concentration Injection S/N RT Ion Ratio Quantifier Qualifier (ppb) volume (ul) (Quantifier) (specify) (specify) Blank (solvent) CC-1-0.05 CC-2-0.1 CC-3-0.15 CC-4-0.3 CC-5-0.45 CC-6-0.6 Remarks: Furnish calibration details including chromatogram. B) Repeatability & Reproducibility Test: Name of analyte: Chloramphenicol Concentration: 0.3ppb 1st Occasion: Date:.................. Start Time:...................End Time:.................. Obtained Area Injection S/N Replicate RT Ion Ratio Quantifier Qualifier volume (ul) (Quantifier) (specify) (specify) Solvent 1st 2nd 3rd 4th 5th 6th 7th Mean (Area) SD (Area) %RSD (Area) 2nd Occasion: Date:.................. Start Time:...................End Time:.................. Obtained Area Injection S/N Replicate RT Ion Ratio Quantifier Qualifier volume (ul) (Quantifier) (specify) (specify) Solvent 1st 2nd 3rd 4th 5th 6th 7th
Annex-IX FORMAT FOR PERFORMACE SHEET LINEARITY, REPEATABILITY & REPRODUCIBILITY TEST A) Linearity details: Name of analyte: Chloramphenicol Date:.................. Start Time:...................End Time:.................. Concentration (ppb) Injection volume (ul) RT Ion Ratio Obtained Area S/N (Quantifier) Quantifier (specify) Qualifier (specify) Blank (solvent) CC-1-0.05 CC-2-0.1 CC-3-0.15 CC-4-0.3 CC-5-0.45 CC-6-0.6 Remarks: Furnish calibration details including chromatogram. B) Repeatability & Reproducibility Test: Name of analyte: Chloramphenicol Concentration: 0.3ppb 1st Occasion: Date:.................. Start Time:...................End Time:.................. Replicate Injection volume (ul) RT Ion Ratio Obtained Area S/N (Quantifier) Quantifier (specify) Qualifier (specify) Solvent 1st 2nd 3rd 4th 5th 6th 7th Mean (Area) SD (Area) %RSD (Area) 2nd Occasion: Date:.................. Start Time:...................End Time:.................. Replicate Injection volume (ul) RT Ion Ratio Obtained Area S/N (Quantifier) Quantifier (specify) Qualifier (specify) Solvent 1st 2nd 3rd 4th 5th 6th 7th
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