Organic Analytes Inorganic Analytes Field/Laboratory sample ID Field/Laboratory sample ID Confirmation of results when positive results are Method reference number(s) (digestion/analysis detected from location not previously tested by where applicable) laboratory Detection & quantitation limits defined Method reference number(s) (extraction/analysis Chain of custody where applicable) Date of analysis Detection & quantitation limits defined Sample receipt and login information Chain of custody Positive controls Date of analysis Matrix spike/matrix spike duplicate Sample receipt and login information Laboratory control sample (LCS) System monitoring compound Negative controls Positive controls Method Blanks Matrix spike/matrix spike duplicate Inductively Coupled Plasma (ICP) interference Laboratory control sample check sample criteria met* Surrogates Post digestion spike sample information Negative controls Method of standard addition (MSA) if applicable Method Blanks Sample preparation details GC/MS tuning - proof of acceptance Pre/post sample amounts Internal standard area and retention time summary Digestions Sample preparation details Dilutions Pre/post sample amounts Sample prep log* Extractions Sample data Sample cleanups Case Narrative Dilutions Raw sample data, instrument output* Sample prep/extraction log Instrument run log* Sample data Initial calibration acceptance criteria* Case Narrative Continuing calibration acceptance criteria* Quantitation reports Accreditation certification if not meeting Chromatographs * exception as defined in 30 TAC§25.6 Spectra * Instrument run log * Initial calibration acceptance criteria met* Continuing calibration acceptance criteria met* Manual integrations with pre and post integration chromatograms* Audit trail report * Accreditation certification if not meeting exception defined in 30 TAC §25.6
Organic Analytes Field/Laboratory sample ID Confirmation of results when positive results are detected from location not previously tested by laboratory Method reference number(s) (extraction/analysis where applicable) Detection & quantitation limits defined Chain of custody Date of analysis Sample receipt and login information System monitoring compound Positive controls Matrix spike/matrix spike duplicate Laboratory control sample Surrogates Negative controls Method Blanks GC/MS tuning - proof of acceptance Internal standard area and retention time summary Sample preparation details Pre/post sample amounts Extractions Sample cleanups Dilutions Sample prep/extraction log Sample data Case Narrative Quantitation reports Chromatographs * Spectra * Instrument run log * Initial calibration acceptance criteria met* Continuing calibration acceptance criteria met* Manual integrations with pre and post integration chromatograms* Audit trail report * Accreditation certification if not meeting exception defined in 30 TAC §25.6 Inorganic Analytes Field/Laboratory sample ID Method reference number(s) (digestion/analysis where applicable) Detection & quantitation limits defined Chain of custody Date of analysis Sample receipt and login information Positive controls Matrix spike/matrix spike duplicate Laboratory control sample (LCS) Negative controls Method Blanks Inductively Coupled Plasma (ICP) interference check sample criteria met* Post digestion spike sample information Method of standard addition (MSA) if applicable Sample preparation details Pre/post sample amounts Digestions Dilutions Sample prep log* Sample data Case Narrative Raw sample data, instrument output* Instrument run log* Initial calibration acceptance criteria* Continuing calibration acceptance criteria* Accreditation certification if not meeting exception as defined in 30 TAC§25.6
FY2011EPAApprovedADAComplianceCopy.docx