Name: ______Justin Date: ___08/27/2014___ Exp. #: Arthur Student__________ JAS-21 Title: _______Isolation of Eugenol from the Steam Distillation of Cloves ____________________________ Purpose: _____ To isolate eugenol from cloves by steam distillation and analyze it using IR _________________and 1H-NMrspectroscopy___________________________________________________________ Chemical & Safety Data: Substance Structure MW (g/mol) m.p. (oC) b.p. (oC) Density (g/mL) Role Name: Dichloromethane 84.93 -97 39 to 40 1.32 Solvent N/A Formula: Safety: CH2Cl2 Irritant, possible cancer hazard, inhalation may cause CNS effects Name: Sodium sulfate 142.04 884 N/A N/A Drying Agent N/A Formula: Safety: Na2SO4 Possible irritant Name: Eugenol 164.20 -12 to -10 254 1.06 Analyte Formula: Safety: C10H12O2 Irritant, potential allergen Name: Chloroform-d 120.38 -64 61 1.5 Solvent N/A Formula: Safety: CDCl3 Irritant, possible cancer hazard, inhalation may cause CNS effects
Name: ______Justin Arthur Student__________ Date: ___08/27/2014___ Exp. #: JAS-21 Title: _______Isolation of Eugenol from the Steam Distillation of Cloves ____________________________ Purpose: _____ To isolate eugenol from cloves by steam distillation and analyze it using IR _________________and 1H-NMrspectroscopy___________________________________________________________ Chemical & Safety Data: Substance Structure MW (g/mol) m.p. (oC) b.p. (oC) Density (g/mL) Role Name: Dichloromethane N/A 84.93 -97 39 to 40 1.32 Solvent Formula: CH2Cl2 Safety: Irritant, possible cancer hazard, inhalation may cause CNS effects Name: Sodium sulfate N/A 142.04 884 N/A N/A Drying Agent Formula: Na2SO4 Safety: Possible irritant Name: Eugenol 164.20 -12 to -10 254 1.06 Analyte Formula: C10H12O2 Safety: Irritant, potential allergen Name: Chloroform-d N/A 120.38 -64 61 1.5 Solvent Formula: CDCl3 Safety: Irritant, possible cancer hazard, inhalation may cause CNS effects
Example%20Technique%20Lab%20Report%20Rev%201-2016.docx