suspected Fill in all necessary information Brownfields QAPP Template #8 Analytical Laboratory Instrument and Equipment Maintenance, Testing, and Inspection Identify all analytical instrumentation that requires maintenance, testing or inspection and provide the SOP reference for each. Document the frequency, acceptance criteria and corrective action requirements on the template. Below (in italics) is an example of such information. Analytical Instrument/ Maintenance Testing/Inspection Acceptance Corrective Responsible Frequency SOP Equipment Activity Activity Criteria Action Person Reference ICP-MS As per instrument As per instrument As per instrument Acceptable Inspect the EPA CLP ILM05.4 recalibration; system, RAS manufacturer’s manufacturer’s manufacturer’s recommendations recommendations; recommendations see ILM05.4 correct Laboratory check connections problem, ICP-MS recalibrate Technician and/or reanalyze samples. Fill in all necessary information Analytical Laboratory Instrument Calibration Identify all analytical instrumentation that requires calibration and provide the SOP reference number for each. Document the frequency, acceptance criteria, and corrective action requirements on the template. Below (in italics) is an example of such information. Instrument/Equipment Calibration Frequency of Acceptance Corrective Responsible Analytical Procedure Calibration Criteria Action Person SOP Reference ICP-MS See ILM05.4; ICP-MS ICP-MS: As ICP-MS: EPA CLP ILM05.4 as per Initial per instrument inspect the RAS instrument calibration: system, Laboratory manufacturer’s daily or once recommended correct ICP-MS manufacturer’s
suspected Fill in all necessary information Brownfields QAPP Template #8 Analytical Laboratory Instrument and Equipment Maintenance, Testing, and Inspection Identify all analytical instrumentation that requires maintenance, testing or inspection and provide the SOP reference for each. Document the frequency, acceptance criteria and corrective action requirements on the template. Below (in italics) is an example of such information. Instrument/ Equipment Maintenance Activity Testing/Inspection Activity Frequency Acceptance Criteria Corrective Action Responsible Person Analytical SOP Reference ICP-MS As per instrument manufacturer’s recommendations As per instrument manufacturer’s recommendations; check connections As per instrument manufacturer’s recommendations Acceptable recalibration; see ILM05.4 Inspect the system, correct problem, recalibrate and/or reanalyze samples. EPA CLP RAS Laboratory ICP-MS Technician ILM05.4 Fill in all necessary information Analytical Laboratory Instrument Calibration Identify all analytical instrumentation that requires calibration and provide the SOP reference number for each. Document the frequency, acceptance criteria, and corrective action requirements on the template. Below (in italics) is an example of such information. Instrument/Equipment Calibration Procedure Frequency of Calibration Acceptance Criteria Corrective Action Responsible Person Analytical SOP Reference ICP-MS See ILM05.4; as per instrument manufacturer’s ICP-MS Initial calibration: daily or once ICP-MS: As per instrument manufacturer’s recommended ICP-MS: inspect the system, correct EPA CLP RAS Laboratory ICP-MS ILM05.4
EPA-Region-2-Brownfields-QAPP-Templates.docx