2.449 2.048 1.799 1.657 mm-1 μ, 188(1) 198(2) 173(1) 173(1) T, K 0.71073 0.71073 0.71073 Å λ, R1 a 0.0206 0.0303 0.0189 0.0203 wR2b 0.0555 0.0706 0.0439 0.0525 = [Σ||Fo|-|Fc||]/[Σ|Fo|] for [Fo2 > 2σ(Fo2)]. = {[Σw(Fo2- a R1 b wR2 Fc2)2]/[Σw(Fo4)]}½. References
μ, mm-1 2.449 2.048 1.799 1.657 T, K 188(1) 198(2) 173(1) 173(1) λ, Å 0.71073 0.71073 0.71073 R1 a 0.0206 0.0303 0.0189 0.0203 wR2b 0.0555 0.0706 0.0439 0.0525 a R1 = [Σ||Fo|-|Fc||]/[Σ|Fo|] for [Fo2 > 2σ(Fo2)]. b wR2 = {[Σw(Fo2- Fc2)2]/[Σw(Fo4)]}½. References
MShaver.docx