obtained for each fortification level were less than [xx]%. Recovery and repeatability data are presented in Tables B.5.2.3-2, below. B.5.2.3-2. Accuracy and Precision Data From the [Method ID] Multiresidue Method. Fortification Validation Recovery (%) RSD Analyte Matrix Level (ppm) (%) Individual Mean Range Analyte 1 Matrix 1 xx xxx→yyy m/z yy (quantitation) zz Analyte 1 Matrix 2 xx xxx→yyy m/z yy (quantitation) zz Analyte 1 Matrix 3 xx xxx→yyy m/z yy (quantitation) zz Analyte 2 Matrix 1 xx xxx→yyy m/z yy (quantitation) zz Analyte 2 Matrix 2 xx xxx→yyy m/z yy (quantitation) zz Analyte 2 Matrix 3 xx xxx→yyy m/z yy (quantitation) zz Analyte 1 Matrix 1 xx xxx→yyy m/z yy (confirmation) zz Analyte 1 Matrix 2 xx xxx→yyy m/z yy (confirmation) zz Analyte 1 Matrix 3 xx xxx→yyy m/z yy (confirmation) zz Analyte 2 Matrix 1 xx xxx→yyy m/z yy (confirmation) zz Analyte 2 Matrix 2 xx xxx→yyy yy m/z (confirmation) zz Analyte 2 Matrix 3 xx xxx→yyy yy m/z (confirmation) zz V. Limit of Quantitation Table B.5.2.3-3. Summary of Detection and Quantitation Limits for the [Method ID] Multiresidue Method. Analyte LOD (ppm)1 LOQ (ppm)2 1 LOD = limit of detection, determined by [explain]. 2 LOQ = limit of quantitation, defined as the lowest fortification level where acceptable precision and accuracy data were obtained.
obtained for each fortification level were less than [xx]%. Recovery and repeatability data are presented in Tables B.5.2.3-2, below. B.5.2.3-2. Accuracy and Precision Data From the [Method ID] Multiresidue Method. Analyte Matrix Fortification Level (ppm) Validation Recovery (%) RSD (%) Individual Mean Range Analyte 1 m/z xxx→yyy (quantitation) Matrix 1 xx yy zz Analyte 1 m/z xxx→yyy (quantitation) Matrix 2 xx yy zz Analyte 1 m/z xxx→yyy (quantitation) Matrix 3 xx yy zz Analyte 2 m/z xxx→yyy (quantitation) Matrix 1 xx yy zz Analyte 2 m/z xxx→yyy (quantitation) Matrix 2 xx yy zz Analyte 2 m/z xxx→yyy (quantitation) Matrix 3 xx yy zz Analyte 1 m/z xxx→yyy (confirmation) Matrix 1 xx yy zz Analyte 1 m/z xxx→yyy (confirmation) Matrix 2 xx yy zz Analyte 1 m/z xxx→yyy (confirmation) Matrix 3 xx yy zz Analyte 2 m/z xxx→yyy (confirmation) Matrix 1 xx yy zz Analyte 2 m/z xxx→yyy (confirmation) Matrix 2 xx yy zz Analyte 2 m/z xxx→yyy (confirmation) Matrix 3 xx yy zz V. Limit of Quantitation Table B.5.2.3-3. Summary of Detection and Quantitation Limits for the [Method ID] Multiresidue Method. Analyte LOD (ppm)1 LOQ (ppm)2 1 LOD = limit of detection, determined by [explain]. 2 LOQ = limit of quantitation, defined as the lowest fortification level where acceptable precision and accuracy data were obtained.