TPR ultimately yields a bulk reduction of the. sample; the peak maxima are an indication of the. reducibility of the metal oxide phase. Careful. observation of Figure 2 shows a small, broad peak at higher temperatures than Tmax. This peak is attributable to the reduction of. some bulk oxide in the sample. The specific. particle size of the sample is an important. experimental variable; in fact, for bulk ox-. ides an increase in Tmax is predicted for an. increasing particle size.
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