Indentation hardness
Hardness measurements quantify the resistance of a material to plastic deformation. Indentation hardness tests compose the majority of processes used to determine material hardness, and can be divided into two classes: "microindentation" and "macroindentation" tests. Microindentation tests typically have forces less than . Hardness, however, cannot be considered to be a fundamental material property. Classical hardness testing usually creates a number which can be used to provide a relative idea of material properties. As such, hardness can only offer a comparative idea of the material's resistance to plastic deformation since different hardness techniques have different scales.
Indentation hardness
Scratch tests at low loads, such as the Bierbaum microcharacter test, performed with either 3 gf or 9 gf loads, preceded the development of microhardness testers using traditional indenters. In 1925, Smith and Sandland of the UK developed an indentation test that employed a square-based pyramidal indenter made from diamond. They chose the pyramidal shape with an angle of 136° between opposite faces in order to obtain hardness numbers that would be as close as possible to Brinell hardness numbers for the specimen. The Vickers test has a great advantage of using one hardness scale to test all materials.The first reference to the Vickers indenter with low loads was made in the annual report of the National Physical Laboratory in 1932. Lips and Sack describes the first Vickers tester using low loads in 1936.
There is some disagreement in the literature regarding the load range applicable to microhardness testing. ASTM Specification E384, for example, states that the load range for microhardness testing is 1 to 1000 gf. For loads of 1 kgf and below, the Vickers hardness (HV) is calculated with an equation, wherein load ("L") is in grams force and the mean of two diagonals ("d") is in millimeters: