mmol 및 디클로로메탄 mls. 시약의 혼합물을 실온에서 2시간 동안 교반했습니다. 반응 후, 용액을 중탄산나트륨 수용액으로 세척하고 회전식 증발기를 사용하여 유기층을 분리하고 고체로 건조시켰습니다.

mmol and dichloromethane mls. The mixture of reagents was stirred at room temperature for two hours. Following the reaction, the solution was washed with aqueous sodium bicarbonate wv and the organic layer was separated and dried to a solid using a rotary evaporator.