NiSb3 is Skutterudite structured and crystallizes in the cubic Im-3 space group. Ni(1) is bonded to six equivalent Sb(1) atoms to form corner-sharing NiSb6 octahedra. The corner-sharing octahedral tilt angles are 54°. Sb(1) is bonded in a 2-coordinate geometry to two equivalent Ni(1) atoms.
NiSb3 is Skutterudite structured and crystallizes in the cubic Im-3 space group. Ni(1) is bonded to six equivalent Sb(1) atoms to form corner-sharing NiSb6 octahedra. The corner-sharing octahedral tilt angles are 54°. All Ni(1)-Sb(1) bond lengths are 2.57 Å. Sb(1) is bonded in a 2-coordinate geometry to two equivalent Ni(1) atoms.