Nd(NiSb)2 crystallizes in the tetragonal I4/mmm space group. Nd(1) is bonded in a 16-coordinate geometry to eight equivalent Ni(1) and eight equivalent Sb(1) atoms. Ni(1) is bonded in a 4-coordinate geometry to four equivalent Nd(1) and four equivalent Sb(1) atoms. Sb(1) is bonded in a 9-coordinate geometry to four equivalent Nd(1), four equivalent Ni(1), and one Sb(1) atom.
Nd(NiSb)2 crystallizes in the tetragonal I4/mmm space group. Nd(1) is bonded in a 16-coordinate geometry to eight equivalent Ni(1) and eight equivalent Sb(1) atoms. All Nd(1)-Ni(1) bond lengths are 3.45 Å. All Nd(1)-Sb(1) bond lengths are 3.41 Å. Ni(1) is bonded in a 4-coordinate geometry to four equivalent Nd(1) and four equivalent Sb(1) atoms. All Ni(1)-Sb(1) bond lengths are 2.50 Å. Sb(1) is bonded in a 9-coordinate geometry to four equivalent Nd(1), four equivalent Ni(1), and one Sb(1) atom. The Sb(1)-Sb(1) bond length is 2.91 Å.