How to turn oil into in a gel? I've seen some EPR experiments where they add gelatin to water with spin-probes in it, as it &quot;hardens&quot; it immobilizes the spin-probes so that you can check effect of tumbling rate on the EPR. Cool
I would like to do the same with asphaltene in crude oil.... So I'm looking for a chemical that I can add to oil that will turn it into a more-or-less solid black gooey mess. It shouldn't be something too reactive though, because I don't want it to change the chemical aspects of the asphaltene (e.g. not make it self-aggregate). Just lock it in place.
Thoughts?
Put your asphaltene source on a silica gel column and elute with hexane and then hexane/toluene mixture to remove paraffins (saturated compounds), aromatics, and resins (small polar compounds). At last, remove the asphaltenes (high molecular weight polar compounds) with pure toluene, evaporate to dryness (a brittle black solid), then with heat you can disolve/disperse the asphaltenes in a simple high molecular weight neutral material like petroleum jelly and let it cool. This will give a high and/or adjustable concentration of what you want to look at. https://en.wikipedia.org/wiki/Asphaltene