When you stop at the Masonic Hotel you can be assured that a beautiful meal or refreshing drink is not far away.
Whether you are after a light snack or a good hearty meal the restaurant has the perfect atmosphere for you.
There is a nice selection of entrées, mains, Stone Grill options, and of course desserts to choose from.
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The STONEGRILL System ensures fast, efficient service and a healthy, nutritious meal with a sensational taste, unique to STONEGRILL.
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The perfect atmosphere can make your drink so much more enjoyable. Whether you are soaking up the heat of the fire in winter or relaxing in the sun on the patio in summer the Masonic Hotel has created the friendly environment where you can do what is best for you.
If you are looking to have a drink in a more private setting you can visit the bottle store!
Have a corporate or informal function you need to organise? Then come and see our friendly staff to discuss your space and catering needs. Vintage car tours are also available for functions upon enquiry.


The astronomical system of units, formally called the IAU (1976) System of Astronomical Constants, is a system of measurement developed for use in astronomy. It was adopted by the International Astronomical Union (IAU) in 1976, and has been significantly updated in 1994 and 2009 (see astronomical constant).
The system was developed because of the difficulties in measuring and expressing astronomical data in International System of Units (SI units). In particular, there is a huge quantity of very precise data relating to the positions of objects within the solar system which cannot conveniently be expressed or processed in SI units. Through a number of modifications, the astronomical system of units now explicitly recognizes the consequences of general relativity, which is a necessary addition to the International System of Units in order to accurately treat astronomical data.
The astronomical system of units is a tridimensional system, in that it defines units of length, mass and time. The associated astronomical constants also fix the different frames of reference that are needed to report observations. The system is a conventional system, in that neither the unit of length nor the unit of mass are true physical constants, and there are at least three different measures of time.
The astronomical unit of time is the day, defined as 7004864000000000000♠86400 seconds. 365.25 days make up one Julian year. The symbol D is used in astronomy to refer to this unit.
The astronomical unit of mass is the solar mass. The symbol M☉ is often used to refer to this unit. The solar mass (M☉), 7030198892000000000♠1.98892×1030 kg, is a standard way to express mass in astronomy, used to describe the masses of other stars and galaxies. It is equal to the mass of the Sun, about 7005333000000000000♠333000 times the mass of the Earth or 1,048 times the mass of Jupiter.
Jupiter mass (MJ or MJUP), is the unit of mass equal to the total mass of the planet Jupiter, 7027189800000000000♠1.898×1027 kg. Jupiter mass is used to describe masses of the gas giants, such as the outer planets and extrasolar planets. It is also used in describing brown dwarfs and Neptune-mass planets.
Earth mass (M⊕) is the unit of mass equal to that of the Earth. 1 M⊕ = 7024597410000000000♠5.9742×1024 kg. Earth mass is often used to describe masses of rocky terrestrial planets. It is also used to describe Neptune-mass planets. One Earth mass is 6997315000000000000♠0.00315 times a Jupiter mass.
The astronomical unit of length is that length for which the Gaussian gravitational constant (k) takes the value 6998172020989500000♠0.01720209895 when the units of measurement are the astronomical units of length, mass and time. The dimensions of k2 are those of the constant of gravitation (G), i.e., L3M−1T−2. The term "unit distance" is also used for the length A while, in general usage, it is usually referred to simply as the "astronomical unit", symbol au, AU or ua.
An equivalent definition of the astronomical unit is the radius of an unperturbed circular Newtonian orbit about the Sun of a particle having infinitesimal mass, moving with a mean motion of 6998172020989500000♠0.01720209895 radians per day. It is approximately equal to the mean Earth–Sun distance.
The speed of light in IAU is the defined value c0 = 7008299792458000000♠299792458Lua error: Unmatched close-bracket at pattern character 67. of the SI units. In terms of this speed, the astronomical unit of length has the presently accepted value: 1 ua = c0τA = 7011149597870700000♠1.49597870700×1011 ± 3 m, where τA is the transit time of light across the astronomical unit. The astronomical unit of length is determined by the condition that the measured data in the ephemeris match observations, and that in turn decides the transit time τA.
The distances to distant galaxies are typically not quoted in distance units at all, but rather in terms of redshift. The reasons for this are that converting redshift to distance requires knowledge of the Hubble constant which was not accurately measured until the early 21st century, and that at cosmological distances, the curvature of space-time allows one to come up with multiple definitions for distance. For example, the distance as defined by the amount of time it takes for a light beam to travel to an observer is different from the distance as defined by the apparent size of an object.
^ a b c d Resolution No. 10 of the XVIth General Assembly of the International Astronomical Union, Grenoble, 1976.
^ In particular, there is the barycentric celestial reference system (BCRS) centered at the barycenter of the solar system, and the geocentric celestial reference system (GCRS) centered at the center of mass of the Earth (including its fluid envelopes) Dennis D. McCarthy, P. Kenneth Seidelmann (2009). "Resolution B1.3: Definition of the barycentric celestial reference system and geocentric celestial reference system XXIVth International Astronomical Union General Assembly (2000)". Time: from Earth rotation to atomic physics. Wiley-VCH. p. 105. ISBN 3-527-40780-4.
^ a b Gérard Petit and Brian Luzum, eds. (2010). "Table 1.1: IERS numerical standards" (PDF). IERS technical note no. 36: General definitions and numerical standards. International Earth Rotation and Reference Systems Service. For complete document see Gérard Petit and Brian Luzum, eds. (2010). IERS Conventions (2010): IERS technical note no. 36. International Earth Rotation and Reference Systems Service. ISBN 978-3-89888-989-6.
^ International Bureau of Weights and Measures (2006), The International System of Units (SI) (PDF) (8th ed.), p. 126, ISBN 92-822-2213-6 .
"2014 Selected Astronomical Constants" in The Astronomical Almanac Online, USNO–UKHO .


For the first time, President Donald Trump directly mocked professor Christine Blasey Ford Tuesday night, posing a series of sarcastic questions to laughter and applause from a Mississippi rally crowd.
"How do you get home? I don't remember. How did you get there? I don't remember. How many years ago? I don't know. I don't know. I don't know. I don't know. What neighborhood was it in? I don't know. Where is the house? I don't know. Upstairs, downstairs, where was it? I don't know," he said.
Though it's not unusual for victims of trauma to forget some logistical details about their attacks, Blasey Ford did actually testify about some of the specifics Trump listed related to her alleged assault, including details about the room where she says it occurred.
"A man's life is shattered. His wife is shattered and his daughters who are beautiful and young kids," he said. "They destroy people, they want to destroy people. These are really evil people," he said, presumably referring to Democrats.


There is a place in Canada where the killer whale population is significantly denser than anywhere else on Earth.
To make matters even better, there is also an abundance of humpback whales, dolphins, sea lions, porpoises,eagles and seals. This place is called the Johnstone Strait and it is situated near the northern tip of Vancouver Island in British Columbia. The strait is dotted with pristine forested islands, on which we will be camping for a full week of photography, whale watching and exploration by kayaks.This unique photography expedition is suitable for people without any previous kayaking experience.We will be paddling in very stable kayaks, and all the gear, water and food that we will need to live on our own in nature for the entire expedition will be stored safely in waterproof hatches. The Johnstone Strait is part of the Inside Passage, located between Vancouver Island and the mainland - and although technically it is in the Pacific Ocean, it is well sheltered from the ocean swell. Our route is a one-way route, carefully chosen in order to see as much as possible of the area, without the need to return to our starting point.The adventure will be led by one of todays top outdoor photographers, Alex Buisse, together with two highly-trained local kayak guides. Given that the group will be formed of no more than six participants, this is an exclusive experience for passionate photographers who want to challenge their creative selves, photograph cetaceans from their kayaks, and immerse themselves in wild nature.
Dates: 23 - 31 July 2015Group size:max 6 (+ 3guides)Accommodation:- base camps/ tent:6nights- hotel:2nightsExpedition leader:Alex BuisseAlex Buisseis an adventure photographer who has spent an unplanned night on an ice face in January, climbed a granite spire alone for four days, named three mountains in Greenland, flown from the summits of snowy peaks, trekked through the wilderness of Tierra del Fuego and kayaked near to sea lions in the Galapagos Islands, among many other adventures. Alex shoots for clients such as Patagonia, RedBull, Sports Illustrated, Black Diamond and the Patagonian Expedition Race. His work has been published in The New York Post, Outdoor Photography, NationalGeographic.com, Alpinist, Climbing, The Telegraph, and many other prestigious publications.
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"You cannot simplyreadthe Quran, not if you take it seriously. You either have surrendered to it already or you fight it. It attacks tenaciously, directly, personally; it debates, criticizes, shames, and challenges. From the outset it draws the line of battle, and I was on the other side. I was at a severe disadvantage, for it became clear that the Author knew me better than I knew myself. The Quran was always way ahead of my thinking; it was erasing barriers I had built years ago and was addressing my queries".


Be there for as long as possible.
If you are doing any SEO and these two are not your top priorities, then you have to sit down, grab a cup of coffee and think!
Now, if you are on Google page #1, position #1 for your hunted keyword, don't celebrate yet. You still have work my dear friend. Pogo-Sticking may be your next enemy to deal with.
The battle for position #1 on page #1 is fierce – keyword research, competition analysis, creating great content, backlinks, etc.
But if you go through these struggles and succeed to push your entries to the most coveted position on SERPs, you have to make sure you don't allow pogo-sticking pull your items off that position.
NB: In this post, I wrote about a little known trick that's guaranteed to remarkably increase your natural traffic. Don't fail to check that article out.
Pogo sticking in SEO is a situation where a user performs a search, clicks on a result and very quickly clicks back to the search result page, and clicks on a different result.
Of course, a negative signal is sent to Google and that makes it think it made a mistake by ranking you on top because you just failed to satisfy the searcher.
If this happens over and over again, Google will seriously consider shifting you down stairs. (Well, Google here represents search engines).
You may get all the tough high PR backlinks and the keyword stuffs to get to position #1 but once searchers start rejecting your content by clicking back to the next entry on SERP, Google is smart enough to think something is seriously wrong with your content.
Given that search engines strive to satisfy their users, you'll soon find your entries moving down to the bottom.
This isn't good at all!
How do you measure your Pogo Sticking Effect?
Well, I have not seen any tool yet to measure your pogo-sticking effect. If you have one, please share with us in the comment box.
However, your bounce rate can be a quick pointer. Note however that high bounce rate doesn't necessary indicate high pogo-sticking. A closer look into these two shows some interesting differences.
The only way to reduce pogo-sticking is to make sure your readers from search engines don't quickly click back to search engine results page (SERP). To do this, you'll have to understand what your readers want and write for them.
You can write for your readers while inviting search engines to send you traffic. The best way of course is to treat a topic in its substantial details with less of focus keyword and more of Latent semantic indexing (LSI) keywords.
LSI keywords is what helps search engines to quickly link up your articles with searchers. Write for your readers but don't neglect SEO.
NB: SEOPressor is an excellent WordPress plugin to automatically scan and create a list of LSI keywords for your posts. All you do then is perfectly insert the keywords in your article.
Readers love a welcoming theme. Fortunately, you don't need to hurt your wallet in today's themes market to be able to own one.
If your blog suffers pogo-picking effect because of poor theme, you are really not thinking straight. I think your theme should be the last thing that throws your visitors off.
There are some premium WordPress themes that are worthless too. A lot of things have to come to table when choosing the right theme for your blog. That's why I always recommend you grab premium themes from the guys of Genesis or MyThemeShop. These have won the confidence and love of their users through high quality products and support services.
Note however that getting the best theme ever does not guarantee any significant reduction in pogo-sticking. Other factors, of course have a place.
Your post title is like a door into your article. Once visitors get attracted, they click to discover what's inside.
Your introduction is the 'Welcome' spot. Once they are not properly welcomed, they may feel they are not at the right place. The next thing is a quick turn-back.
Your post introduction should be as important as the title. There must be a perfect correlation or connection between your title, introduction and of course body.
Many of your readers skim across your content. One of the things that keep them on your content are the headlines. As they scroll down your page, they quickly read through your headlines to get a general idea of what's in the content. If you fail to catch their attention through catchy headlines, you stand the risk of pogo-sticking.
One of the things readers cannot escape are beautiful and attractive images. Using relevant and eye-catching, appealing or striking pictures or screenshots on your post will have a positive impact on your blog's pogo-sticking and bounce rate.
Once someone is attracted to an image, he tends to find out what's more about it by trying to read the text surrounded it, hence, more time on your blog and a possible Click-through.
The worst thing to do to your blog is to mislead your readers. They will go away and you're never going to see them around your blog again.
Don't title your article as a way to lure readers to click. Once they find out your content is completely away from your title, they'll click back in anger.
Many bloggers use popups these days to capture leads but it's a stupid error to setup your popup window to pup on PageLoad.
While this quickly drives many readers away, it helps to add to your pogo-sticking. If your popup plugin doesn't allow you to delay your popup window, you should seriously consider switching to something more professional.
To achieve more results, your window should popup once your reader makes an attempt to leave the page or once a certain position on the page is scrolled to.
An example is, when a reader scrolls to the comment box or simply when the reader spends x minutes on your blog. This helps you capture targeted leads while reducing your pogo-sticking.
If you find your article today on Google page #1 and tomorrow it's off, you should pay attention to these points I have mentioned. There may be other factors though. However pogo-sticking is one factor you should not neglect.
I'll be excited to hear from you in the comment box. Let me know what you think about pogo-picking and your SEO.
Kindly share this post with your friends on social media or link to it from your posts.
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There are a number of great reasons to purchase your prescriptions online. Aside from the pure convenience, you can also enjoy easier comparison shopping and ultimately, lower prices. Some utilize online prescription services to avoid the perceived embarrassment of physically picking up certain medications. There are a number of compelling reasons to order medication online, you just need to be careful to utilize a service that is trustworthy and dependable. You can easily find information to safely order medication from a Canadian or other international online pharmacy.


Using a 22-point lead as buffer to ride out a furious finish by the enemy on Sunday night, San Miguel Beer scored a 99-91 victory over Barangay Ginebra that put the Beermen back on track in the 2019 PBA Philippine Cup at Smart Araneta Coliseum.
five points heading into the final 1:30.
It was a great way for San Miguel to bounce back after taking a shock loss to Columbian last week, and the sharpness that the Beermen played with for at least 90% of the way clearly reestablished them as–as what has been the case for several years now–the team to beat in the season's most prestigious conference.
San Miguel is seeking to win this conference for the fifth straight year, and in the pre-season was ballyhooed to run away with it after acquiring Terrence Romeo in a blockbuster trade from TNT KaTropa.
But after that unexpected loss to the Dyip with Romeo playing, it certainly didn't pass as a good start for the Beermen, until they came out against the Kings–with Romeo in civilian clothes because of an injury–to change all that.
Ginebra 91 – Tenorio 24, Aguilar 20, Slaughter 11, Thompson 9, Devance 6, Teodoro 6, Dela Cruz 4, Ferrer 4, Caguioa 3, Mariano 2, Mercado 2.
Quarters: 20-17, 44-35, 78-57, 99-91.


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BRING THE KIDS, BRING THE DOG, YOU'RE ALL WELCOME HERE AT TYRE CITY !


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Racism Suit against Tesla by Employee
November 15, 2017 Jeffrey
Tesla is one of the leading companies when it comes to innovation in the technology of cars. However, it seems that the company is still operating in the pre- Civil rights era according to some of the workers present there.Marcus Vaughn, an African American employee of the company has recently filed a law suit on behalf of him and a group of workers who accuses the company to be a racist one. According to Mr. Vaughn, there are over 100 workers in Tesla who have been harassed in the company and seeks monetary as well as reform compensation from the same due to the bad working conditions and lack of policies against racial harassments.
While Mr. Vaughn tried to bring this to the notice of the human resource department and Elon Musk himself, he was terminated with the excuse of lacking a positive attitude in the work environment. Mr. Vaughn also states that the supervisors and colleagues often used the "N word" apart from other racial discrimination acts.While there has been no official reaction from the side of Tesla on this suit being filed in the Alameda County Superior Court of California, Mr. Elon Musk has sent an email to the employees of Tesla stating that it is not right to demean a historically less represented group but sometimes the actions aren't intentional and that in cases where the wrong doer apologizes, the victim should be a bit thick skinned and accept it.
The suit was filed by California Civil Rights Law Group and as stated by Larry Organ, an attorney at the firm, Mr. Vaughn approached them when he heard about another suit that the firm had filed on behalf of yet another African American group who brought similar charges against Tesla. Mr. Organ also stated in an interview that Tesla, as a company, wasn't doing enough for the diverse workforce they had. He also said that the company should have taken steps to ensure that all members of their diverse work force felt equally at ease while working in there.
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March 13, 2018 March 15, 2018 Carolyn Farrell
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March 18, 2018 Jeffrey
US Suicide Rates Soar High; Require New Depression Drugs
June 11, 2018 Carolyn Farrell

redpajama_set_name: RedPajamaCommonCrawl


This Safety Plan for Stearns County was prepared as part of the Minnesota statewide highway safety planning process.
better positioning the county to compete for available safety funds.
The Plan includes a description of the connection to safety planning efforts at the national, State (through Minnesota's Strategic Highway Safety Plan and the Highway Safety Improvement Program) and regional (all of the counties in Area Transportation Partnership 3) levels.


Jun 29, 2015· FLADDER denibbing machines for lacquer sanding of solid wood, veneer, painted work pieces and MDF.
DeNibbing and Brush. ... The Alpha-Brush Victory is the perfect machine for sanding linear profiles made of wood, metal, plastic or composites. The machine can be supplied in different configurations like TS, TB, TSB & TSSB depending on application (see brochure).The mac..
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Sanding finishing machine / linear / for wheel rims - CVS - Cefla . ... DeNibbing and Brush - Taurus Craco. We offer a wide variety of denibbing and brush sanders. . The Alpha-Brush Victory is the perfect machine for sanding linear profiles made of wood, metal, Contact Us.


1Birjand University of Technology, Department of Chemical Engineering, P.O. Box 97175/569, Birjand, Iran.
2Birjand University of Technology, Department of Mechanical Engineering, P.O. Box 97175/569, Birjand, Iran.
In the current investigation, Fe3O4 water-based nanofluids were synthesized to examine the effect of an alternative 3-D external magnetic field on its thermal behavioral pattern. A solvothermal method was used to prepare the magnetite nanoparticles. To characterize the nanoparticles, the study employed transmission electron microscopy, X-ray diffraction, Fourier transform infrared spectroscopy, vibrating sample magnetometer and zeta-potential experiments. Vibrating sample magnetometer evaluations thoroughly confirmed the super-paramagnetic characteristics of the nanoparticles. Therefore, exposition of the resulting nanofluids to an AC external magnetic field led to the formation of aligned dipoles parallel to the applied field. Afterwards, the net magnetization in the absence of the external field was set to zero. Thermal measurements demonstrated an enhancement of convective heat transfer coefficients, particularly in the case of more diluted samples. The highest value of h was associated with the most diluted sample, where the h value was two times greater than that in the base fluid at V=1.4 V. This was attributed to the augmentation of both the Brownian motions and the viscosity gradients in the centerline of the test section.


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Best Jrpgs 2020
Final Fantasy VII Remake's release is being treated as a real mainline entry to arguably the biggest JRPG franchise, and as such there's an unmistakable level of hype surrounding it. The waiting time After years of rumours and anticipation, one of the most beloved JRPGs of all time is finally being reimagined This open-world action-adventure seems to be combining the best elements of a world It wouldn't be an exaggeration to say that Final Fantasy VII Remake is one of the most anticipated games of 2020 JRPG purists might balk at the idea of turning Final Fantasy VII into an action RPG
The game has yet to attract a concrete release date, but it's slated for release in 2020. SEGA released three Streets of Rage titles between 1991 and 1994 for the Mega Drive/Genesis, and are widely Final Fantasy VII Remake's release is being treated as a real mainline entry to arguably the biggest JRPG franchise, and as such there's an unmistakable level of hype surrounding it. The waiting time After years of rumours and anticipation, one of the most beloved JRPGs of all time is finally being reimagined This open-world action-adventure seems to be combining the best elements of a world
Best Jrpgs 2020 – It wouldn't be an exaggeration to say that Final Fantasy VII Remake is one of the most anticipated games of 2020 JRPG purists might balk at the idea of turning Final Fantasy VII into an action RPG The game has yet to attract a concrete release date, but it's slated for release in 2020. SEGA released three Streets of Rage titles between 1991 and 1994 for the Mega Drive/Genesis, and are widely TEXT_9
Updated: April 8, 2019 at 11:00 pm
◀ Best Android Emulator 2020
Best Woocommerce Themes 2020 ▶


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Apple's mini 18W USB-C charger may be real after all
By Malcolm Owen | 2 years ago
Rumors of a more powerful 18-Watt USB-C wall charger supposedly being bundled with this fall's iPhone releases have been bolstered, with the surfacing of photographs appearing to depict an engineering sample of the alleged accessory.
Photographs published by Chongdiantou and spotted by Macotakara show the charging plug from three different angles. Along with showing the side and plug prongs in one shot, a second simply shows the USB-C connection at the top of the device, where the USB-C to Lightning connector would be inserted.
The third photograph is blurry but readable, showing it to be an engineering sample. At the bottom the output data claims it can provide up to 5 Volts of power at 3 Amps, equating to 15 Watts delivered to the iPhone, or for 9V to be delivered at 2A, namely 18W.
While this is one of the first credible photographs of the rumored charger, there is no guarantee that it is genuine. A May report included alleged renderings of the European version of the iPhone charger, again offering 18W of power.
Currently, iPhones ship with the same 5W USB-A charger, despite the iPhone 8, iPhone 8 Plus, and iPhone X all supporting Fast Charging, using a USB-C to Lightning cable and a charger with a higher wattage. Fast Charging allows an iPhone to charge to 50 percent of capacity within 30 minutes, which is currently possible using the USB-C wall charger supplied with the MacBook or MacBook Pro, albeit at a relatively high cost.
If Apple does include a USB-C charger with future iPhones, it could also allow third-party accessory producers to create more cables. Apple currently does not allow other vendors to create USB-C to Lightning cables under the MFi certification program, but this stands to change if the rumored charger is included in the iPhone package.
Prototype iPhone 5s shown in black and slate gray colors
FBI investigates Capitol attack iPhone data & school iPad recoveries in the Apple Crime Blotter
melgross Said:
As the batteries in the iPhone and iPad have increased over the years, the only concession to that was going from 10 Watts to 12 Watts for the iPad. Fortunately, we've bought so many iPads over the years, that we never use the iphone 5 watt chargers. I've got a bunch in a draw, and give them away to people who lose their chargers.
i bought the 29 watt Macbook charger along the long cable for it, but it's not a real solution for most people because it costs $49 for that charger, and cost, when I bought it, $39 for the long Lightning to USB C cable.
sometimes Apple takes years to do something they obviously needed to do.
nunzy Said:
Why should Apple give these away for free when they can make a good margin selling them? I guess they think that they will sell enough of additional iPhone to make up the profit and even make some more.
MplsP Said:
You could ask the same question about including headphones or even make the argument not to include an adapter or cable at all because 'virtually everyone has one already and this let's people only pay for what they need.'
Apple sells premium phones at a premium price. As such, I don't expect to get a crippled, underpowered adapter that doesn't take advantage of the phone's capabilities. It's kind of like paying for first class and then having the flight attendant saying you need to pay for a drink.
Why couldn't they do fast charging with USB A? The big problem with switching to a USB C to lightning cable is that it would be incompatible with virtually every charging port in the world right now without an adapter. (Although based on the lack of USB A ports in the MacBooks, convenience & compatibility are not high on Apples list of priorities.)
Eric_WVGG Said:
It's about time.
Because it would be stupid to sell them. Apple's charging times have been behind most Android phones for years. There's no excuse for that, particularly at the prices. Those chargers were used with the first iPhone 10 years ago. The batteries are several times as large in the big models, and so charging times have gotten longer.


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Science & the Arts
The Art of the Score: The Mind, Music, and Moving Images
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Alec Baldwin is joined by the Coen brothers and renowned guests from the worlds of filmmaking, film music, and science to explore the uniquely powerful role of music in shaping the narrative flow and the emotional impact of film. From Stanley Kubrick's classic 2001: A Space Odyssey to the Coen brothers' Fargo and True Grit, this program examines the creative process of scoring feature films and the neuro-scientific insights that reveal how such compositions profoundly shape the audience experience. A Co-Presentation of World Science Festival and the New York PhilharmonicLearn More
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TOPICS: Art & Science, Science in Society
TAGS: 2013, Alec Baldwin, Aniruddh D. Patel, Carter Burwell, coen brothers, Fargo, Joel and Ethan Coen, New York City, NYC, science of music and the score, Stanley Kubrick, The Art of the Score, The Mind Music and Moving Images
PLAYLISTS: Science & the Arts
Video Duration: 01:34:15
Original Program Date: Saturday, September 21, 2013
Moderator: Alec Baldwin
Participants: Carter Burwell, Joel and Ethan Coen, Aniruddh D. Patel
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TOPICS: Art & Science, Biology & Origins of Life, Earth & Environment, Kavli, Mind & Brain, Physics & Math, Science in Society, Science Unplugged, Space & The Cosmos, Technology & Engineering, Youth & Education
TAGS: 2013, Alec Baldwin, Aniruddh D. Patel, Carter Burwell, coen brothers, Fargo, Joel and Ethan Coen, New York City, NYC, science of music and the score, Stanley Kubrick, The Art of the Score, The Mind Music and Moving Images, 2013, Alec Baldwin, Aniruddh D. Patel, Carter Burwell, coen brothers, Fargo, Joel and Ethan Coen, New York City, NYC, science of music and the score, Stanley Kubrick, The Art of the Score, The Mind Music and Moving Images
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Justia Patents Contacting Gas Or Vapor With Solid Sorbent To Store Gas Or VaporUS Patent for Drying device and method for producing the same Patent (Patent # 6,871,419)
Drying device and method for producing the same
Mar 9, 2000 - LTS Lohmann Therapie-Systeme AG
The invention relates to a flat and activable drying device for reducing the moisture content of a gas space surrounding said device and to a method for producing a device of this type. The inventive drying device contains a flat matrix with at least one regenerable drying agent.
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The invention is directed to a device capable of reducing the moisture content, and/or ensuring a defined moisture content, in a closed gas space surrounding said device, to a process for producing such a device, and to the use of said device.
Such drying devices are known in the prior art. They can comprise desiccant-filled containers which are used, for example, for dry storage of moisture-sensitive products.
A desiccant pouch is known which is available commercially under the name Desimax™ from the company Multiform Desiccant Inc. (Buffalo, New York). This type of desiccant pouch consists of two pouch walls which enclose an interior space by means of weld seams at the edge of the pouch walls. Said interior space contains a defined amount of desiccant, namely 4 Å molecular sieve. The pouch walls themselves are at least partly permeable to water vapor.
The disadvantage of such a system is that the defined, limited amount of desiccant present in the pouch interior space corresponds to only a defined, limited moisture absorption capacity. If the amount of desiccant is exhausted by attainment of the maximum absorption capacity for moisture (i.e., essentially water), the desiccant pouch remains ineffective. Further absorption of moisture/water is impossible, and nor is it possible to ensure a constant atmospheric humidity, in particular a reduced atmospheric humidity, in a closed gas space surrounding said desiccant pouch.
In the processing of such desiccant pouches, therefore, the problem occurs that prolonged contact (for example, several minutes) with the ambient air, which generally contains more than 40% relative atmospheric humidity, must be avoided, since otherwise rapid exhaustion occurs, so rendering the desiccant pouch unusable for its subsequent utility in, for example, the production of packaging for moisture-sensitive products. A solution to this problem is either to carry out processing in rooms with constant, greatly reduced relative atmospheric humidity which are closed to the outside, or to accelerate the processing steps which are performed during contact with the ambient air.
In addition, desiccant pouches are not very multifaceted in terms of their usefulness for different drying needs, since the amount of desiccant per pouch (and thus the maximum moisture/water absorption capacity) is limited by the internal volume.
A further disadvantage of desiccant-filled pouches is that the desiccant is present within such a pouch in a solid, usually granulated or powdered form. At the filling stage, therefore, there is first of all a need for very precise metering of the desiccant during the production process. However, when such a system comes under relatively severe mechanical stress, there is a risk that the pouch wall or the weld seam at the edge of the pouch will tear open and that the desiccant will exit. Where the desiccant is not harmless, or may enter into chemical reactions with the product that is to be stored under reduced and/or defined moisture content conditions in a surrounding, closed gas space, therefore, a desiccant pouch of this kind also constitutes a certain safety risk for said product.
DE 196 46 048 discloses packaging for transdermal therapeutic systems, having internally fixed drying devices. This desiccant-containing packaging comprises multilayer laminates. With the aid of a pressure-sensitively adhesive layer, a desiccant layer present therein can be fastened to the assembly comprising the other layers of the laminate. Like the desiccant pouch already described, this packaging is also subject to the rapid exhaustion of the moisture/water absorption capacity in the case of prolonged contact with normal ambient air. By normal ambient air is meant air which does not have a reduced relative atmospheric humidity but instead has at least 40% relative atmospheric humidity. Consequently, processing of these packaging laminates likewise requires process steps within a room closed off with respect to the environment, and/or working in a room with reduced reduced atmospheric humidity.
It is an object of the present invention to provide a device for reducing the moisture content of a closed gas space surrounding said device, or for establishing a defined relative atmospheric humidity, which avoids these disadvantages of the drying devices known in the prior art. The intention is in particular to avoid the need for processing and/or storage beforehand in a closed gas space of reduced moisture content surrounding the device, and/or processing under conditions which are extremely limited in terms of time.
This object is achieved by means of a drying device which comprises a matrix with a desiccant present in it and which can be activated under industrially relevant conditions. If desired, the drying device may include a water-vapor-permeable layer. The matrix can, if desired, be lined directly with this layer. The desiccant comprises a regenerable desiccant. The drying device of the invention and, in particular, the desiccant matrix are preferably in sheet form. In one particular embodiment, the desiccant matrix of said drying device is or has a pressure-sensitively adhesive layer.
For the purposes of the invention, the matrix is a carrier for the desiccant Suitable materials for said matrix are in principle organic and inorganic materials, especially polymeric materials. The matrix materials must possess the capacity to admit the penetration of water molecules into the material and the migration of these molecules within the material. On the other hand, this incoming water must not result in complete dissolution of the polymeric material. Examples of suitable materials are polymeric substances such as acrylates, silicones, polyisobutylenes, SIS rubber, SBS rubber, SEBS rubber, polyvinylpyrrolidone, polyurethane, polyesters, polyethylene, polyvinyl alcohol, polyamides, ethylene-vinyl acetate, polyacrylic acid, Kollidon (copolymer of vinyl acetate and vinylpyrrolidone), and cellulose derivatives. In principle, any film-forming materials can be used. It is of course also possible to use mixtures of the organic polymer materials mentioned. The matrix is free from pharmaceutical active substances.
The matrix is preferably in sheet form. This means that in the spatial conformation of this matrix the three dimensions (height, length and width) are in defined proportions with respect to one another. The height of the sheet-form matrix has a minimum value of about 50 μm and a maximum value of about 3 mm; the height of the sheet-form matrix is preferably between 200 and 500 μm.
The width and length of the sheet-form matrix are not critical parameters, but can be adapted to the practical requirements in each case. Approximately 2 mm can be regarded as a minimum value of the width for practical handleability of the sheet-form matrix. The width of the sheet-form matrix is preferably between about 1 and about 50 cm, with particular preference between about 2 and about 10 cm.
Like the width, the length of the sheet-form matrix can likewise in theory be infinite. For the reason of more simple handleability, preferred lengths are likewise between about 1 and about 50 cm, with particular preference between about 2 and about 10 cm. In one embodiment the desiccant matrix is elastic, by which is understood the capacity for the matrix to exhibit a reversible change of shape. This results in an improvement in certain properties of the matrix, for example, the softness, the pliability, the flexibility and the machineability. For this purpose it is necessary to add substances to the matrix that are able to influence said properties. Such substances include plasticizers (elasticizers) for the respective matrix materials. Examples of suitable plasticizers are polyethylene glycol, polypropylene glycol, glycerol, Miglyol, propanediol, triglycerides, esters such as diethyl phthalate, tributyl citrate, etc., which are added to the matrix if desired in amounts such that the desired elasticity is obtained. This is of course dependent in particular on the nature of the respective matrix material and on the nature of the respective plasticizer, although the other constituents of the desiccant matrix may also have certain influences on the elasticity, so that it is not possible to specify exact limits for the quantitative proportions. Preferably, however, quantitative proportions of from about 1 to 40% plasticizer are present in the matrix (based on the overall weight of the matrix).
In another embodiment the desiccant matrix can be pressure-sensitively adhesive, by which is meant the ability for the matrix, once pressed onto a surface with a certain pressure, to be permanently bonded to said surface. For this purpose it may be necessary to add substances to the matrix which influence this property. Such substances include tackifiers (tackifier resins). Appropriate tackifiers are known to the skillled worker: examples are rosin esters and hydrogenated esters of rosin, hydrocarbon resins, etc., which are added, if desired, to the matrix in amounts such that the desired pressure-sensitive adhesive property is obtained. When choosing the amount of tackifier it is necessary to take account of the specific matrix materials. Here again, the other constituents of the desiccant matrix may have influences on the pressure-sensitive adhesion property, and so it is not possible to specify exact limits for the quantitative proportions. The ranges of amounts are therefore in general between about 5 and 70% tackifier in the matrix. Preferably, quantitative proportions of from about 10 to 30% tackifier are present in the matrix (based on the overall weight of the matrix).
In the embodiment in which the drying device comprises a pressure sensitively adhesive layer, or, even, where the desiccant matrix itself is pressure-sensitively adhesive, said drying device judiciously includes an abhesive backing layer (release liner) which covers this pressure-sensitively adhesive layer and from which the drying device is peeled off prior to its use. The materials for such backing layers are known to the skilled worker and can, for example, comprise films containing substances such as polyethylene terephthalate, polyethylene, polypropylene, paper, and modifications thereof.
As already mentioned, the drying device may further comprise a water vapor-permeable layer. If desired, the matrix can be lined with this layer. The water-vapor-permeable layer can be present on one or both sides of the sheet-form matrix. Appropriate materials for a water-vapor-permeable protective layer of this kind are, for example, cellulose in the form of film, nonwoven, paper, perforated film, etc.
In a further embodiment, the drying device may also include a support layer. The purpose of this layer is to give the drying device greater dimensional stability. This may be the case, for example, when the desiccant matrix itself, owing to very low thickness or relatively high elasticity, is too flexible for practical handleability. The support layer can, if desired, line the matrix or may even be identical with the water-vapor-permeable layer. The support layer can be on one or both sides of the sheet-form matrix. Appropriate materials for such a support layer are materials known to the skilled worker, such as PET film, polyethylene, polypropylene, paper, nonwovens, etc.
If desired, the drying device may also include a protective layer which is intended to protect the desiccant matrix against external mechanical stress, e.g., abrasion, or against the exit of desiccant. If desired, this layer can be identical with the water-vapor-permeable layer and/or with the support layer. Appropriate materials for the protective layer are materials known to the skilled worker, e.g., polymers such as polyethylene, polypropylene, paper, nonwovens, etc.
It is possible for the drying device to include a layer which fulfills at least two of the technical functions of water-vapor-permeable layer, support) layer, and protective layer.
If desired, the desiccant matrix may also include a moisture indicator whose color depends on the water content and which thus indicates whether the desiccant present in the matrix is still capable of further absorption of water. Examples of suitable moisture indicators of this type are copper(II) salts or cobalt(II) salts such as CUSO4 or CoCl2, for example.
For the purposes of the invention, a desiccant is a substance which is able to absorb moisture, but especially water. The ability of such substances to absorb moisture may be based on a chemical or physical effect. Regenerable desiccants—i.e., substances capable under certain conditions of releasing absorbed moisture (for example water) again and thereby undergoing transition to a state in which the substance is capable of renewed moisture absorption—are particularly suitable for the invention. Appropriate regenerable desiccants are CaSO4 (calcium sulfate, anhydrous gypsum, anhydrite), CaSO4.½H2O (hemihydrate), CaCl2, Al2O3, CaO, Na2SO4, K2CO3, CuSO4, Mg(ClO4)2, MgSO4, silica gel (blue indicator gel), polyvinylpyrrolidone (PVP), and mixtures of at least two of these substances.
In accordance with the invention, these substances are used as solids or as a solution. The physical form is not particularly important: it may comprise crystals, powders, amorphous solids, granules, triturated forms, etc. However, the size of these desiccant solids is limited by the requirements for the thickness of the sheet-form matrix. An upper limit for the size of the solid particles is therefore about 200 μm; however, preference is given to the use of particles having a grain size below 50 μm. The minimum grain size of these particles is 1 μm.
The amount of desiccant in the matrix depends primarily on the desired moisture/water absorption capacity of the drying device in question and on the moisture/water absorption capacity of the particular desiccant used.
If, for example, only a low water absorption capacity is required, the use of a desiccant of low water absorption capacity in a small amount in the desiccant matrix may be sufficient. A small amount of desiccant (in active form) close to the lower limit, in the matrix might represent, for example, from about 0.5 to 5% of the overall weight of the desiccant matrix. In that case, the thickness and surface area of the desiccant matrix may even be situated at the respective lower limits.
Where the required water absorption capacity of the drying device is very high, however, it is necessary to use a desiccant matrix containing a relatively large amount of desiccant, the desiccant as well being required to possess a high water absorption capacity. A large amount of desiccant (in active form) of this kind may represent, for example, from about 50 to 70% of the overall weight of the desiccant matrix.
The drying device as such is activatable. This means that the article in its entirety, but of course in particular the desiccant matrix, is stable with respect to the conditions under which the desiccant present in the matrix is regenerated. There must be no irreversible decomposition of individual components or permanent deformation owing, for example, to instances of material softening. This is ensured by using materials which possess resistance to increased temperatures, thermal radiation, or microwaves.
The actual activation of the drying device, or of the desiccant matrix, can be done by various means. The most simple type of activation is to store the desiccant matrix under increased temperature (for example, at 105, 110, 120, 140 or 170° C.) for a defined period. The higher the chosen temperature, the shorter the required storage period. Other possibilities for activation can consist in the use of infrared radiation or microwave irradiation.
As additional measures, a reduced external pressure (for example 0.2 atm) and/or an artificially generated air circulation may facilitate the chosen activating conditions (for example, temperature, duration, radiation intensity). The application of these additional measures may also mean that in the case of increased-temperature activation this temperature need not be above 100° C., the boiling point of water under standard conditions, but may even be from about 60 to 80° C.
As a result of activation, the regenerable desiccant undergoes transition to its active form, in which it possesses the capacity to absorb moisture/water.
It is clear that when choosing the activation method, which may also consist in a combination of different activation methods and additional measures, it is necessary to take account of the materials present in each case in the drying device and/or in the desiccant matrix and of the properties of said materials (sensitivity to infrared or microwave radiation and/or increased temperatures). Otherwise, it may be necessary to adapt the materials of the desiccant matrix and/or of the drying device to the required activating conditions. In addition, it may be necessary to adapt the economy of the activation method to the material costs of the drying device.
Specific embodiments of a desiccant matrix are sheet-form systems, by which are meant, for example, labels, films, tapes, rolls, stickers, or disks.
The advantages of the drying device of the invention are, inter alia, that the desired moisture/water absorption capacity of the drying device can be adapted to the particular need by means of simple calculation of its surface area and, if appropriate, of its thickness and of the concentration of the desiccant in the matrix. This is based on the fact that the water absorption capacity of the drying device, at constant thickness and constant concentration of desiccant in the matrix, is generally in a linear correlation with its surface area. If the water absorption capacity of a drying device used is exhausted, a greater drying requirement might be able to be supplemented by simply adding an additional, readily calculable surface area to the drying device of the invention.
The drying device of the invention is used to reduce the moisture content of a closed gas space surrounding said device or to maintain a defined, preferably a reduced, moisture content in a closed gas space surrounding said device. It can therefore be utilized in a method of reducing the moisture content of a closed gas space surrounding said device or of maintaining a defined, preferably a reduced, moisture content in a closed gas space surrounding said device.
Said gas space must be gastightly closed so that there can be no exchange with ambient air and the atmospheric humidity from the surroundings which it contains. Closed gas spaces of this kind may be, for example, airtight packaging of products.
The possibilities for application of the drying device of the invention are therefore located within the field of the packaging of moisture-sensitive articles, such as, for example, foods, drugs, diagnostic agents, medicaments, moisture-sensitive chemicals, and biologically activatable material. Preference is given to the use of drying devices of the invention within packaging for tablets, transdermal therapeutic systems, and sheet-form form pharmaceutical administration forms for oral use.
Where the desiccant present in the matrix possesses the ability to bind molecules of substances other than water (i.e., for example, organic solvents such as ethanol, methanol, etc., odorous substances such as acetaldehyde, acetic acid, etc., gaseous substances such as CS2, NH3, H2S etc.), a target utility can consist in reducing the amount of such molecules in the gas space surrounding the drying device and/or in keeping said gas space substantially free from such molecules.
The production and performance of the drying device of the invention will be elucidated on the basis of the following examples.
347.84 g of 2-propanol are mixed with
46.36 g of polyethylene glycol 400 and
81.4 g of Kollidon 90 and the mixture is homogenized with stirring.
127.5 g of calcium sulfate ×2H2O are introduced and the mixture is homogenized at high stirring speed.
The resultant, solvented desiccant composition is coated onto a 23 μpolyester film so as to give, following evaporation of the solvent, a desiccant layer of 200 g/m2. The open side of the desiccant layer is laminated with a 26 g/m2 paper. Punched specimens measuring 10 cm2 are produced and are activated at 100° C. for 5 hours.
81.4 g of Kollidon 90 and the mixture is homogenized.
127.5 g of calcium sulfate ×2H2O are introduced into the homogeneous solution, and the mixture is homogenized at high stirring speed.
The resultant, solvented desiccant composition is coated onto a 23μ polyester film so as to give, following evaporation of the solvent, a desiccant layer of 200 g/m2. In a separate coating operation, the commercial pressure-sensitive adhesive Durotak 387-2287 (manufacturer: National Starch & Chemical) is coated onto a single-sidedly abhesive polyester film so as to give, following evaporation of the solvent, a pressure-sensitive adhesive coat of 20 g/m2. The open side of the pressure-sensitive adhesive coat is laminated with the polyester side of the desiccant coat. Punched specimens measuring 10 cm2 are produced and are activated at 105° C. for 5 hours.
Five each of the punched specimens produced by the processes described in Example 1 and in Example 2 are subjected to a test to determine the water absorption capacity. For this purpose, following initial activation in a desiccator, the punched specimens were stored over supersaturated calcium nitrate solution ( 55% relative humidity) for at least 24 hours. The water absorption which has taken place is determined by weighing the punched specimens at defined intervals of time.
After 24 hours, there was a slow decrease in the water absorption capacity of these specific drying devices. The punched specimens were reactivated under the conditions specified in Example 1 and, respectively, in Example 2 and were subjected to a second test to determine the water absorption capacity.
Table 1 shows the results of these experiments on the water absorption of the drying devices of the invention. It can be ascertained that the water absorption takes place continuously over a period of at least 24 hours.
TABLE 1 1 hour 2 hours 4 hours 6 hours 24 hours
Water absorption (mg) {overscore (X)} n = 5 after storage
Example 1 6.90 10.10 12.22 13.72 17.64 Example 2 4.74 7.28 9.38 11.38 15.52
Water absorption after reactivation (mg) {overscore (X)} n = 5 after storage
Example 1 7.30 8.78 10.28 10.98 14.78 Example 2 6.62 8.28 10.30 11.14 15.18
The drying capacity of the drying device of the invention is therefore not restricted (as in the case of the prior art drying devices) to one-off and/or short-duration drying.
The experiment of Example 3 also shows, however, that the drying device of the invention can be used to perform a method of reducing the moisture content of a closed gas space and/or maintaining a reduced moisture content of a closed gas space, which comprises in a first step converting an activatable drying device, comprising a sheet-form matrix having at least one regenerable desiccant, by activation into the active state, in a further step placing the activatable drying device in the active state into the gas space whose moisture content is to be reduced and/or whose reduced moisture content is to be maintained, in a further step airtightly closing said gas space with respect to the surroundings; finally, in a further step, the activatable drying device in the active state absorbs moisture from the airtightly closed gas space over a prolonged period of, for example, at least one hour.
FIG. 1 shows different embodiments of the activatable drying device of the invention. The different elements are explained in the attached legend. The figure depicts:
1=activatable drying device consisting of a desiccant matrix.
2=activatable drying device consisting of a desiccant matrix and a support layer.
3=activatable drying device consisting of a release liner, a fixing 1=, means, a support layer, and a desiccant matrix.
4=activatable drying device consisting of a release liner, a desiccant matrix, and an underlying support layer.
5=activatable drying device consisting of a desiccant matrix surrounded by two support layers.
6=activatable drying device consisting of the assembly of release liner, a fixing means, and a desiccant matrix surrounded by two support layers.
FIG. 12 demonstrates an embodiment of an activatable drying device according to the invention.
1. An adhesive, activatable sheet-form drying device, comprising:
a desiccant polymeric matrix containing a regenerable desiccant agent therein and having pressure-sensitive adhesive properties;
a support layer disposed on one side of said matrix; and
a release liner disposed on the other side of said matrix wherein the support layer is water-vapor-permeable.
2. The adhesive, activatable sheet-form drying device according to claim 1, wherein the polymeric matrix comprises at least one polymeric material selected from the group consisting of acrylates, silicones, polyisobutylens, SIS rubber, SEBS rubber, polyvinylpyrrolidone, polyurethane, polyesters, polyethylene, polyvinylalcohol, polyamides, ethylene-vinylacetate, polyacrylic acid, kollidon and cellulose derivatives thereof.
3. The adhesive, activatable sheet-form drying device according to claim 1, wherein the regenerative desiccant is selected from the group consisting of CaSO4, CaSO4½H2O, CaCl2, Al2O3, CaO, Na2SO4, K2CO3, CuSO4, Mg(ClO4)2, MgSO4, silica gel and polyvinylpyrrolidone.
4. The adhesive, activatable sheet-form drying device according to claim 1, wherein the water-vapor-permeable layer comprises a material selected from the group consisting of paper, cellulose, nonwovens and perforated films.
5. The adhesive, activatable sheet-form drying device according to claim 1, wherein the release liner comprises a material selected from the group consisting of films containing polyethylene terephthalate, polyethylene, polypropylene, paper and modifications thereof.
6. The adhesive, activatable sheet-form drying device according to claim 1, wherein the polymeric matrix further comprises one or more plasticizers selected from the group consisting of polyethylene glycol, polypropylene glycol, glycerol, miglyol, propane diol, triglycerides, diethyl phthalate and tributyl citrate.
7. The adhesive, activatable sheet-form drying device according to claim 1, wherein the polymeric matrix further comprises one or more tackifiers selected from the group consisting of rosin esters, hydrogenated rosin esters and hydrocarbon resins.
8. The adhesive, activatable sheet-form drying device according to claim 1, wherein the polymeric matrix further comprises a moisture indicator selected from the group consisting of copper (II) salts and cobalt (II) salts.
9. The adhesive, activatable sheet-form drying device according to claim 8, wherein the desiccant comprises solid particles having a size from 1 to 50 μm.
10. The adhesive, activatable sheet-form drying device according to claim 1, wherein the desiccant comprises solid particles having a size of from 1 to 200 μm.
11. An adhesive, activatable sheet-from drying device, comprising:
a desiccant polymeric matrix containing a regenerable desiccant therein;
a support layer disposed on one or both sides of said matrix;
a pressure-sensitive adhesive layer; and
a release liner covering said pressure-sensitive adhesive layer wherein one or both support layer, art water-vapor-permeable.
12. The adhesive, activatable sheet-form drying device according to claim 11, wherein the polymeric matrix comprises at least one polymeric material selected from the group consisting of acrylates, silicones, polyisobutylens, SIS rubber, SEBS rubber, polyvinylpyrrolidone, polyurethane, polyesters, polyethylene, polyvinylalcohol, polyamides, ethylene-vinylacetate, polyacrylic acid, kollidon and cellulose derivatives thereof.
13. The adhesive, activatable sheet-form drying device according to claim 11, wherein the regenerative desiccant is selected from the group consisting of CaSO4, CaSO4½H2O, CaCl2, Al2O3, CaO, Na2SO4, K2CO3, CuSO4, Mg(ClO4)2, MgSO4, silica gel and polyvinylpyrrolidone.
14. The adhesive, activatable sheet-form drying device according to claim 11, wherein the water-vapor-permeable layer comprises a material selected from the group consisting of paper, cellulose, nonwovens and perforated films.
15. The adhesive, activatable sheet-form drying device according to claim 11, wherein the support layer comprises a material selected from the group consisting of polyethylene terephthalate, polyethylene, polypropylene, paper and nonwovens.
16. The adhesive, activatable sheet-form drying device according to claim 11, wherein the release liner comprises a material selected from the group consisting of films containing polyethylene terephthalate, polyethylene, polypropylene, paper and modifications thereof.
17. The adhesive, activatable sheet-form drying device according to claim 11, wherein the polymeric matrix further comprises one or more plasticizers selected from the group consisting of polyethylene glycol, polypropylene glycol, glycerol, miglyol, propane diol, triglycerides, diethyl phthalate and tributyl citrate.
18. The adhesive, activatable sheet-form drying device according to claim 11, wherein the polymeric matrix further comprises one or more tackifiers selected from the group consisting of rosin esters, hydrogenated rosin esters and hydrocarbon resins.
19. The adhesive, activatable sheet-form drying device according to claim 11, wherein the polymeric matrix further comprises a moisture indicator selected from the group consisting of copper (II) salts and cobalt (II) salts.
20. The adhesive, activatable sheet-form drying device according to claim 11, wherein the desiccant comprises solid particles having a size of from 1 to 200 μm.
21. The adhesive, activatable sheet-form drying device according to claim 20, wherein the size of the solid particles is from 1 to 50 μm.
22. A method of reducing moisture content and/or maintaining a reduced moisture content in a closed gas space surrounding a drying device comprising the steps of:
a) converting an activatable drying device as claimed in claim 1 or 11 by activation into an active state;
b) placing the activated drying device obtained according to step a) above into the gas-space whose moisture content is to be reduced and/or whose reduced moisture content is to be maintained;
c) airtightly closing said gas space with respect to the surroundings.
23. The method according to claim 22, wherein a closed gas space is formed by an air tight packaging of moisture-sensitive articles.
24. The method according to claim 23, wherein the moisture-sensitive articles are selected from the group consisting of tablets, transdermal therapeutic systems and sheet-form pharmaceutical administration forms for oral use.
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Filed: Mar 9, 2000
Date of Patent: Mar 29, 2005
Assignee: LTS Lohmann Therapie-Systeme AG (Andernach)
Inventors: Franz-Josef Becker (Neuwied), Robert-Peter Klein (Neuwied)
Primary Examiner: Kenneth Rinehart
Attorney: Frommer Lawrence & Haug LLP
Current U.S. Class: Contacting Gas Or Vapor With Solid Sorbent To Store Gas Or Vapor (34/416); 34/DIG.001; Absorption/adsorption Of Gas Or Vapor Released From Treated Material (34/472); Regeneration Of Absorption/adsorption Material (34/473)


text:
Lebo M Back With His Third Wife
Lebohang Morake, affectionately known as Lebo M has reportedly rekindles his love with third wife, Angela Ngani-Casara. This according to reports by Sowetan Live, which also reveals that The Lion King producer will be documenting his relationship with ex-wife and more on his new reality show, Lebo M – Coming Home.
This comes months after it was reported that Lebo M and fiance Malefu "Mel" Ntsala have split in January before they were set to tie the knot. His wedding to Mel would have been the playwright's fifth marriage.
Other reports claim that Lebo and Angela got back together in March this year and she has moved in with he and his 90-year-old mother along with his four kids in his equestrian estate in Blair Atholl, Centurion.
His 10-part reality series which will premiere on Showmax in November 2020, promises to give viewers a clear view of what the composer is about. He will be working on fixing his relationship with his eldest children, the death of his 9th child and will also detail how he overcame his alcohol addiction as he celebrates 15 years of sobriety.
According to Showmax he will be mending his broken relationship with four of his children, Zakiya, Nthabiseng and Refi who are currently based in the US, and his son who lives in the country. He too has become a father.
The four children he lives with include five-year-old daughter Lulo whose mother is Zoe Mthiyane from Generations: The Legacy and his nine-year-old daughter Letti who he had with Angela Ngani-Casara, along with her teenage children Mthuzi and Ketso, which she has in her previous relationships
Speaking to Sowetan Live he explains how sceptical he was about doing a reality series but wanted to tell his story his way. "I was initially sceptical about a reality show, but having recently learnt no-one really knows who I really am in South Africa, my beloved home country of birth. I've become romantic about opening up and having my fans and audience here hang out with Angela and my children via this conversation in 10 episodes," he explained.
After he and Mel split up, she told Sunday World that she was aware that Angela was back in his life, "The wedding was supposed to have happened this year but no, it didn't happen. I thought he is back with Angela, what happened?"
Reason for their split was that they grew apart from each other, "I mean really, there is really nothing I can say. He was a good person, he was a good partner, he was an amazing partner but we had to be where we are today and I'm so… I'm happy for him. "We were both tired of each other. You know relationships, we decided that you know what, this is not good for us. This not for us," said Mel.
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Why can't some COVID-19 vaccinated people travel to the US?
Photo: AP Illustration/Peter Hamlin.
Created: November 18, 2021 08:15 AM
Why can't some COVID-19 vaccinated people travel to the U.S.?
Because they might not be vaccinated with shots recognized by the U.S. Food and Drug Administration or the World Health Organization.
When lifting overseas travel restrictions in November, the U.S. required adults coming to the country to be fully vaccinated with shots approved or authorized by the FDA or allowed by WHO.
Among the most widely used vaccines that don't meet that criteria are Russia's Sputnik V vaccine and China's CanSino vaccine. Sputnik V is authorized for use in more than 70 countries while CanSino is allowed in at least nine countries. WHO still is awaiting more data about both vaccines before making a decision.
Vaccines recognized by the FDA and WHO undergo rigorous testing and review to determine they're safe and effective. And among the vaccines used internationally, experts say some likely won't be recognized by the agencies.
"They will not all be evaluated in clinical trials with the necessary rigor," said Dr. William Moss, executive director of the Johns Hopkins International Vaccine Access Center.
An exception to the U.S. rule is people who received a full series of the Novavax vaccine in a late-stage study. The U.S. is accepting the participants who received the vaccine, not a placebo, because it was a rigorous study with oversight from an independent monitoring board.
The U.S. also allows entry to people who got two doses of any "mix-and-match" combination of vaccines on the FDA and WHO lists.
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Q: Whenever I creating a new project, the xcode window will disapper Whenever I creating a new project, the xcode(4.2) downloaded from MacStore, the xcode window will disapper in os x lion
and when I open any project, it will displaying me this window!

A: I can't really tell what the problem might be from your question, other than perhaps XCode is crashing. If Xcode is no longer running after this, then it's crashing. Completely uninstall XCode and re-download and install it.
http://www.youtube.com/watch?v=GOB3P2XzmiI&v=GOB3P2XzmiI&gl=US

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