glycol and diethyleneglycol monoethyl ether acetate were obtained from fluka chemicals limited glossop england ethyl hydroxy ethyl cellulose high viscosity grade was purchased from polysciences inc warrington u s a all other chemicals were of reagent grade i weight 133 6 mg ttf aldrich in to a glass universal bottle in 30 ml capacity and add approximately 5 ml diethyl ether fluka ii weigh 2 g t 10 graphite morganite into a large high sided glass petri dish iii add the ttf dissolved in diethyl ether to the graphite wash out any remaining ttf from the universal bottle with approximately 4 ml diethyl ether and add the washings to the graphite iv in a fume hood mix the ttf and graphite using a spatula until all the diethyl ether has evaporated and the ttf is deposited on to the graphite v weight 536 mg god glucox ps sturge into a straight sided wide necked screw top jar 100 ml capacity add 4 67 g of a two percent w v aqueous solution of hydroxy ethyl cellulose hec fluka containing six percent w v ethylene glycol fluka and mix to dissolve the god vi mix the graphite ttf into the god solution and rotate on an angled 45 u00b0 rotary mixer at 4 rpm for two to three hours at room temperature a for dimethyl ferrocene dmf the above precedure was repeated but dmf was substituted weight for weight for ttf b for tetracyanoquinodimethane tcnq the above procedure was repeated but substituting tcnq for ttf in a weight for weight manner in addition the tcnq was.