water phasewater deionized 73 11methyl paraben u s p 0 15sodium sulfite 0 4p phenylenediamine 0 84 chlororesorcinol 0 054 chloro m phenylenediaminesulfate 0 04titanium dioxide 0 25glycerol 4 0perfume 0 15______________________________________ after combination of the oil and water phases at a temperature of 60 u00b0 to 70 u00b0 c the product is cooled to 45 u00b0 50 u00b0 c and perfume is added the product is then cooled to room temperature and immediately packed into airtight containers and topped with nitrogen to prevent premature oxidation ______________________________________ percent byphase ingredient weight______________________________________a mixture of cetearyl alcohol and ceteareth 20 6 00a self emulsifying propylene glycol monostearate 5 potassium stearate 4 00a carnation oil 65 75 11 00a propyl paraben 0 05b deionized water 73 15b methyl paraben 0 15b sodium sulfite 0 40c p phenylenediamine 0 80c 4 chlororesorcinol 0 05d titanium dioxide 328 0 25d glycerin 96 4 00e perfume 0 15 total 100 00______________________________________ 1 in a stainless steel jacketed kettle equipped with agitation combine ingredients of phase a and heat to 75 u00b0 c 2 in a separate vessel combine ingredients of phase b and heat to 80 u00b0 c 4 place phase b under a blanket of nitrogen and slowly add phase c maintain heat and continue mixing until dyestuffs are completely dissolved 5 in another vessel sprinkle titanium dioxide in glycerin extending slowly until completely dispersed phase d 9 cool to 30 u00b0 c and fill into lined aluminum tubes this preparation is a white odorless emulsion which is stable in metal tubes the hair coloring preparation which constitutes this invention comprises the following components a an oil in water emulsion of 5 to 20 parts by.