9 u00b0 114 5 u00b0 33 34 33 9 fmoc gln 100 82 100 223 4 u00b0 221 3 u00b0 18 10 17 0 fmoc met 93 78 100 133 4 u00b0 129 132 u00b0 29 24 28 3 fmoc trp 98 5 93 100 182 3 u00b0 165 6 u00b0 27 76 26 6 fmoc asp otbu 91 8 87 100 149 152 148 9 u00b0 22 54 20 3 fmoc leu 92 3 86 100 153 4 u00b0 153 4 u00b0 25 33 24 1 fmoc ile 94 4 88 100 148 9 u00b0 145 7 u00b0 12 44 11 9 fmoc glu otbu 94 86 100 82 4 u00b0 76 7 u00b0 1 27 0 8 sup dfmoc lys boc 91 84 100 132 4 u00b0 123 4 u00b0 11 93 11 7 fmoc ser tbu 100 93 100 128 131 u00b0 126 9 u00b0 26 08 25 4 sup dfmoc asn 99 89 sup e 187 8 u00b0 185 6 u00b0 11 85 11 4 fmoc cys stbu 97 3 65 sup e 75 8 u00b0 74 6 u00b0 82 88 84 6 sup dfmoc thr tbu 100 89 sup e 133 4 u00b0 129 132 u00b0 5 47 4 5 fmoc tyr tbu 90 85 100 150 1 u00b0 150 1 u00b0 27 34 27 6 __________________________________________________________________________ sup a determined by ion exchange chromatography on a beckman 121m amino acid analyzer sup b literature values 3 in parentheses sup c in dimethylformamide c l except where indicated sup d in ethyl acetate sup e not determined by amino acid analysis oligomeric standards not available homogeneous by tlc ______________________________________abbreviations ______________________________________tms trimethylsilyl ch sub 3 sub 3 si tms cl trimethylsilylchloride ch sub 3 sub 3 siclfmoc 9 fluorenylmethyloxycarbonyldipea.