Investigation of a lithium-halogen exchange flow process for the preparation of boronates by using a cryo-flow reactor.Conducting low-temperature organometallic reactions under continuous flow conditions offers the potential to more accurately control exotherms and thus provide more reproducible and scalable processes.  On moving to a continuous system, thermocouple measurements have been used to track exotherms and provide a level of safety for continuous processing of organometallic reagents. 
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