Characterization of cellulose I/II hybrid fibers isolated from energycane bagasse during the delignification process: Morphology, crystallinity and percentage estimation.Cellulose I, cellulose II and cellulose I/II hybrid fibers were prepared from energycane bagasse using NaOH and NaClO2 treatments.  The definitive defibrillation effect with an average width of 12±5μm was observed for the fibers treated with 20wt% NaOH for 10h and NaClO2 for 2h.  The ribbon shaped cellulose I fibers were converted to a swollen state with a rougher surface by 20wt% NaOH treatment for 10h. 
NaOH
Characterization of cellulose I/II hybrid fibers isolated from energycane bagasse during the delignification process: Morphology, crystallinity and percentage estimation.Cellulose I, cellulose II and cellulose I/II hybrid fibers were prepared from energycane bagasse using NaOH and NaClO2 treatments.  The definitive defibrillation effect with an average width of 12±5μm was observed for the fibers treated with 20wt% NaOH for 10h and NaClO2 for 2h.  After further NaClO2 treatment, the CI values were decreased because of partial destruction of hydrogen bond network. 
NaClO2
XRD, NMR and FTIR results present the same trend in the degree of crystallization for all the samples.
XRD
XRD, NMR and FTIR results present the same trend in the degree of crystallization for all the samples.
NMR
XRD, NMR and FTIR results present the same trend in the degree of crystallization for all the samples.
FTIR